1,2,3,4,5,6,7,8-八氢菲合成路线 （共 80 条）
反应条件
cobalt-oleate; manganese-oleate; oxygen
T=60 - 80°C;
参考文献
Schroeter
Patent: DE568338 , 1927 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 19, p. 769,771
反应条件
chromic acid; acetic acid
参考文献
Riedel,J. D.
Patent: DE397150 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 460
Full Text Show Details
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
参考文献
Riedel,J. D.
Patent: DE397150 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 460
Full Text Show Details
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
aluminium trichloride
参考文献
van de Kamp; Mosettig
Journal of the American Chemical Society, 1935 , vol. 57, p. 1107,1109
反应条件
1: phosphorus pentoxide / 175 °C
2: alkali; sodium hypochlorite
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
nachfolgend Zersetzen mit Eis und Salzsaeure;
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
potassium permanganate; manganese(II) sulphate tetrahydrate; 4-laurylbenzenesulfonic acid sodium salt in water
T=95°C; 50 h; PressureTemperatureSolventReagent/catalystTime;
参考文献
Ida, Ryoji; Yanagawa, Shinichiro
Patent: US2014/18569 A1, 2014 ;
Location in patent: Paragraph 0114 ;
反应条件
1: aluminium chloride / 80 °C
2: bei der Zinkstaubdestillation
3: nickel catalyst; tetralin / 120 - 150 °C / 7600 - 15200 Torr / Hydrogenation
4: nickel; tetralin / 180 °C / 10640 Torr / Hydrogenation
5: chromium trioxide; glacial acetic acid
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
1: aluminium chloride / 80 °C
2: bei der Zinkstaubdestillation
3: nickel catalyst; tetralin / 120 - 150 °C / 7600 - 15200 Torr / Hydrogenation
4: nickel; tetralin / 180 °C / 10640 Torr / Hydrogenation
5: chloroform; bromine
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
1: aluminium chloride / 80 °C
2: bei der Zinkstaubdestillation
3: nickel catalyst; tetralin / 180 - 200 °C / Hydrogenation
4: Cr2O3-H2SO4
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
