N-环己基-4-甲基苯甲酰胺合成路线 (共 15 条)
反应条件
in methanol
T=20°C; 24 h;
参考文献
Shaabani, Ahmad; Soleimani, Ebrahim; Rezayan, Ali Hossein
Tetrahedron Letters, 2007 , vol. 48, # 35 p. 6137 - 6141
反应条件
n-butyl-sec-butylmagnesium
1.) n-heptane, 1h, reflux, 2.) methylene chloride, 65 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Sanchez, Ramiro; Vest, Gary; Despres, Lisa
Synthetic Communications, 1989 , vol. 19, # 16 p. 2909 - 2914
反应条件
aluminium trichloride
参考文献
Effenberger,F.; Gleiter,R.
Chemische Berichte, 1964 , vol. 97, p. 472 - 479
反应条件
in acetonitrile
T=25°C; competition reaction with cyclohexylamine, methanol and/or further alcohol; alcoholysis and aminolysis of aroylazide; dependence of amide formation on the kind of alc. solvent or amine; Product distributionMechanism;
参考文献
Ulbricht, Mathias; Boehme, Peter; Hartmann, Udo
Monatshefte fuer Chemie, 1993 , vol. 124, # 11/12 p. 1149 - 1156
反应条件
in cyclohexane
T=25°C; various solvents and concentrations; half life time; ΔH(excit.), ΔS(excit.); Rate constantKineticsThermodynamic data;
参考文献
Ulbricht, Mathias; Boehme, Peter; Hartmann, Udo
Monatshefte fuer Chemie, 1993 , vol. 124, # 11/12 p. 1149 - 1156