N-环己基-4-甲基苯甲酰胺合成路线 （共 15 条）
反应条件
1: 1-(iodo)-4-methylbenzene; cyclohexylamine With sodium carbonate in water
0.166667 h; Autoclave;
2: carbon dioxide in water
T=100°C; P=5171.62 Torr; 8 h; Autoclave;
参考文献
Qureshi, Ziyauddin S.; Revankar, Santosh A.; Khedkar, Mayur V.; Bhanage, Bhalchandra M.
Catalysis Today, 2012 , vol. 198, # 1 p. 148 - 153
反应条件
trifluoromethylsulfonic anhydride; triethylamine; triphenyl-phosphine oxide in 1,2-dichloro-ethane
T=25°C; 0.25 h;
参考文献
Hendrickson, James B.; Hussoin, Md. Sajjat
Journal of Organic Chemistry, 1989 , vol. 54, # 5 p. 1144 - 1149
反应条件
palladium diacetate; triethylamine in water
T=100°C; P=5171.62 Torr; 8 h; Autoclave;
参考文献
Tambade, Pawan J.; Patil, Yogesh P.; Bhanushali, Mayur J.; Bhanage, Bhalchandra M.
Synthesis, 2008 , # 15 art. no. P04608SS, p. 2347 - 2352
反应条件
tris(2,4-di-tert-butyl-phenyl) phosphite; potassium methanolate; [Ni(O2CCH3)2]*4H2O in diethylene glycol dimethyl ether
T=110°C; 10 h;
参考文献
Jo, Youngshin; Ju, Jinhun; Choe, Jaehoon; Kwang, Ho Song; Lee, Sunwoo
Journal of Organic Chemistry, 2009 , vol. 74, # 16 p. 6358 - 6361
反应条件
4 A molecular sieve; hydrogen; triethylamine; palladium on activated charcoal
T=120°C; P=46543.3 Torr; 24 h;
参考文献
Lin, Yong-Shou; Alper, Howard
Angewandte Chemie - International Edition, 2001 , vol. 40, # 4 p. 779 - 781
反应条件
samarium in acetonitrile
T=20°C; 2 h;
参考文献
Shi, Feng; Li, Jian; Li, Chunju; Jia, Xueshun
Tetrahedron Letters, 2010 , vol. 51, # 46 p. 6049 - 6051
反应条件
sodium carbonate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) in water
T=170°C; 0.166667 h; microwave irradiation;
参考文献
Wu, Xiongyu; Larhed, Mats
Organic Letters, 2005 , vol. 7, # 15 p. 3327 - 3329
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane
T=160°C; 0.333333 h; Microwave irradiation;
参考文献
Odell, Luke R.; Saevmarker, Jonas; Larhed, Mats
Tetrahedron Letters, 2008 , vol. 49, # 42 p. 6115 - 6118
反应条件
copper(l) iodide; di-tert-butyl peroxide; 4,7-Dimethoxy-1,10-phenanthroline in benzene
T=100°C; 24 h; Inert atmosphere;
参考文献
Tran, Ba L.; Li, Bijie; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2555 - 2563
反应条件
dipotassium peroxodisulfate; palladium diacetate; silver nitrate in water; dimethyl sulfoxide; acetonitrile
T=70°C; 0.166667 h;
参考文献
Li, Mingzong; Wang, Cong; Fang, Ping; Ge, Haibo
Chemical Communications, 2011 , vol. 47, # 23 p. 6587 - 6589
