偶氮苯-4,4'-二甲酸二甲酯合成路线 （共 11 条）
反应条件
polymethylhydrosiloxane; palladium on activated charcoal in ethanol T=20°C; 5 h;
参考文献
Chandrasekhar; Raji Reddy; Jagadeeshwar Rao
Synlett, 2001 , # 10 p. 1561 - 1562
反应条件
1: With indium trifluoromethanesulfonate; triethylsilane in N,N-dimethyl-formamide
T=60°C; 5 h;
2: With oxygen in N,N-dimethyl-formamide
T=60°C; 15 h;
参考文献
Sakai, Norio; Fujii, Kohji; Nabeshima, Shinya; Ikeda, Reiko; Konakahara, Takeo
Chemical Communications, 2010 , vol. 46, # 18 p. 3173 - 3175
反应条件
sodium azide in N,N-dimethyl-formamide
T=150°C; 2 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Logue, Marshall W.; Han, Byung Hee
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1638 - 1642
反应条件
1: 15 percent Spectr. / dimethylformamide / 0.02 h / 97 °C
2: 6 percent Spectr. / NaN3 / dimethylformamide / 1 h / 150 °C
View Scheme
参考文献
Logue, Marshall W.; Han, Byung Hee
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1638 - 1642
反应条件
chromic acid; acetic acid
参考文献
Meyer,F.; Dahlem
Justus Liebigs Annalen der Chemie, 1903 , vol. 326, p. 337
参考文献
Meyer,F.; Dahlem
Justus Liebigs Annalen der Chemie, 1903 , vol. 326, p. 337
反应条件
methanol
1.) reflux; Yield given. Multistep reaction;
参考文献
Patel, Dalpat I.; Smalley, Robert K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2587 - 2590
反应条件
pyridine; sulfuric acid; acetic acid
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Shimao, Ichiro; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 2 p. 643 - 644
反应条件
pyridine; sulfuric acid
Yield given. Multistep reaction;
参考文献
Shimao, Ichiro; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 2 p. 643 - 644
参考文献
Korschak; Winogradowa
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 154,161; engl. Ausg. S. 138, 143
