(3Z,13Z)-3,13-十八碳二烯-1-基乙酸酯合成路线 （共 52 条）
反应条件
sodium acetate T=0°C;
参考文献
Narasimhan; Ganeshwar Prasad; Madhavan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 2 p. 99 - 101
反应条件
1: H2, quinoline / Pd-BaSO4 / hexane 2: 98 percent / NaOAc / 0 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 35, # 2 p. 99 - 101
反应条件
hydrogenchloride in tetrahydrofuran
反应条件
pyridine in tetrahydrofuran 1) -20 deg C, 0.5 h, 2) r.t., 3 h;
参考文献
Bestmann; Zeibig; Vostrowsky
Synthesis, 1990 , # 11 p. 1039 - 1047
反应条件
1: NaNH2 / tetrahydrofuran / 3 h 2: tetrahydrofuran / 0 - 20 °C 4: H2, quinoline / Pd-BaSO4 / hexane 5: 98 percent / NaOAc / 0 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 35, # 2 p. 99 - 101
反应条件
toluene-4-sulfonic acid in pyridine Heating;
参考文献
Yamamoto, Akira; Ishihara, Toshinobu; Fukumoto, Takehiko
Agricultural and Biological Chemistry, 1989 , vol. 53, # 1 p. 285 - 288
反应条件
1: 99 percent / PPTS / diethyl ether / 4 h / 60 °C 2: H2 / Pd/CaCO3 poisoned with Pb / hexane / 18 h 3: pyridine; DMAP View Scheme
参考文献
Tetrahedron, , vol. 60, # 45 p. 10239 - 10244
反应条件
1: 57 percent / p-toluenesulfonic acid / methanol / 4 h / 60 °C 2: 91 percent / H2, quinoline / Pd/CaCO3 / hexane 3: 82 percent / pyridine / CH2Cl2 / 5 h / Ambient temperature View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 69, # 2 p. 103 - 105
反应条件
sodium hexamethyldisilazane in tetrahydrofuran 1. -78 deg C, 1h 2. 25 deg C, 20h;
参考文献
Vinczer, Peter; Baan, Gabor; Novak, Lajos; Szantay, Csaba
Tetrahedron Letters, 1984 , vol. 25, # 25 p. 2701 - 2704
反应条件
1: tetrahydrofuran / 0 - 20 °C 3: H2, quinoline / Pd-BaSO4 / hexane 4: 98 percent / NaOAc / 0 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 35, # 2 p. 99 - 101
