1: bis-diphenylphosphine With copper(l) iodide; N-methyl-2-(methylamino)ethylamine in toluene 2: 1-iodo-2-methoxybenzene With caesium carbonate in toluene T=110°C; 20 h;
参考文献
Gelman, Dmitri; Jiang, Lei; Buchwald, Stephen L.
Organic Letters, 2003 , vol. 5, # 13 p. 2315 - 2318
1: methoxybenzene With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; cobalt(II) dibromide in tetrahydrofuran; hexane T=0 - 20°C; 0.5 h; 2: chloro-diphenylphosphine in tetrahydrofuran; hexane T=20°C; 3: With water in tetrahydrofuran; hexane
in tetrahydrofuran; methanol 96 h; Inert atmosphereMolecular sieveReflux;
参考文献
Li, Jie; Lutz, Martin; Spek, Anthony L.; Van Klink, Gerard P.M.; Van Koten, Gerard; Klein Gebbink, Robertus J.M.
Journal of Organometallic Chemistry, 2010 , vol. 695, # 24 p. 2618 - 2628
