1: ethyl (2-methyl-2-propenyl)-propanedioate With sodium hydride in tetrahydrofuran; mineral oil
T=20°C; 0.5 h;
2: allyl bromide in tetrahydrofuran; mineral oil
T=20°C; 24 h;
参考文献
Hensle, Eva M.; Tobis, Jan; Tiller, Joerg C.; Bannwarth, Willi
Journal of Fluorine Chemistry, 2008 , vol. 129, # 10 p. 968 - 973
Doran; Shonle
Journal of the American Chemical Society, 1937 , vol. 59, p. 1625
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E.Lilly and Co.
Patent: US2237265 , 1938 ;