1,4-二氨基-2-甲氧基苯合成路线 （共 12 条）
反应条件
sodium hypochlorite in water
参考文献
Hodnett; Prakash
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 2 p. 101 - 104
反应条件
1: 92 percent / pyridine / 1 h / 0 °C 2: 1) sodium 2-nitrobenzenesulfate, FeSO4*7H2O, H2SO4, 2) H2SO4 / 1) 98 deg C, 1 h then 140 deg C, 1 h, 2) 70 - 90 deg C then 133 deg C, 4 h 3: 82 percent / 96percent H2SO4, 90percent HNO3 / 2 h / 96 °C View Scheme
参考文献
Bonhote, Pierre; Wrighton, Mark S.
Synlett, 1997 , vol. 1997, # 8 p. 897 - 898
反应条件
platinum(IV) oxide; hydrogen
16 h;
参考文献
Kumar, Anup; Gupta, Rinkoo D.; Gupta, Tarkeshwar
RSC Advances, 2013 , vol. 3, # 2 p. 390 - 393
反应条件
sodium hydroxide
0.5 h;
参考文献
Bonhote, Pierre; Wrighton, Mark S.
Synlett, 1997 , vol. 1997, # 8 p. 897 - 898
参考文献
Kumar, Anup; Gupta, Rinkoo D.; Gupta, Tarkeshwar
RSC Advances, 2013 , vol. 3, # 2 p. 390 - 393
反应条件
sodium hydroxide; zinc
参考文献
Kumar, Anup; Gupta, Rinkoo D.; Gupta, Tarkeshwar
RSC Advances, 2013 , vol. 3, # 2 p. 390 - 393
参考文献
Am. Cyanamid
Patent: US4137310 , 1979 ;
Chem.Abstr., 1979 , vol. 90, # 186634
反应条件
sodium hypobromide in water
参考文献
Hodnett; Prakash
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 2 p. 101 - 104
反应条件
1: glycerol; as2O5; H2SO4
2: aqueous HBr
View Scheme
参考文献
CIBA
Patent: DE834996 , 1951 ;
DRP/DRBP Org.Chem.
Full Text Show Details
CIBA
Patent: US2640830 , 1950 ;
反应条件
diarsenic pentoxide; sulfuric acid; glycerol
参考文献
Bonhote, Pierre; Wrighton, Mark S.
Synlett, 1997 , vol. 1997, # 8 p. 897 - 898
