6-溴-2-甲基-1,3-苯并噻唑合成路线 (共 20 条)
反应条件
1: With copper(l) iodide; Na2S*9H2O in N,N-dimethyl-formamide T=80°C; 12 h; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 23 p. 4222 - 4225
反应条件
CaO; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene in N,N-dimethyl-formamide T=60°C; 1 h;
参考文献
Chemistry Letters, , p. 839 - 840
反应条件
iron (III) acetylacetonate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether T=20°C; 2.5 h;
参考文献
EP2351744 A1, ;
Page/Page column 71 ;
反应条件
pyridine; antimony(III)tribromide; phenyltrimethylammonium tribromide in dichloromethane T=20°C; 48 h; regioselective reaction;
参考文献
Heterocycles, , vol. 83, # 6 p. 1267 - 1274
反应条件
in methanol 24 h; Irradiation;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, p. 930 - 934
反应条件
in methanol 18 h; Irradiation;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, p. 930 - 934
反应条件
1: 63 percent / P2S5 / benzene / Heating 2: 62 percent / methanol / 24 h / Irradiation View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, p. 930 - 934
反应条件
1: 75 percent / P2S5 / benzene / Heating 2: 23 percent / methanol / 18 h / Irradiation View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, p. 930 - 934
反应条件
1: Br2 / acetic acid / Ambient temperature 2: aq. HCl / Heating View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 30, p. 13 - 17
反应条件
pyridinium tribromide in water
参考文献
Heterocycles, , vol. 83, # 6 p. 1267 - 1274