甲基2,3,4-三-O-苄基-α-D-吡喃葡萄糖苷合成路线 （共 88 条）
反应条件
1.1: NaH / dimethylformamide / 0.33 h / 20 °C 1.2: 15 g / dimethylformamide / 2 h 2.1: 20 percent / HBr / acetic acid / 0.03 h / 15 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 7 p. 1207 - 1214
反应条件
triethyslilane; copper(II) bis(trifluoromethanesulfonate) in dichloromethane; acetonitrile T=20°C; 2 h;
参考文献
Francais, Antoine; Urban, Dominique; Beau, Jean-Marie
Angewandte Chemie - International Edition, 2007 , vol. 46, # 45 p. 8662 - 8665
反应条件
[(BnS)(NO)2Fe]2; tetrabutylammomium bromide; potassium hydride in tetrahydrofuran; ethanol T=40°C;
参考文献
Dieskau, Andre P.; Plietker, Bernd
Organic Letters, 2011 , vol. 13, # 20 p. 5544 - 5547
反应条件
acetic acid T=40°C; 5.5 h;
参考文献
Ramirez, Fausto; Mandal, Sukhendu B.; Marecek, James F.
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2008 - 2013
反应条件
ethylenediamine in methanol T=20°C; 8 h;
参考文献
Temperini, Andrea; Minuti, Lucio
Tetrahedron Letters, 2012 , vol. 53, # 22 p. 2709 - 2711
反应条件
samarium diiodide; water; isopropylamine in tetrahydrofuran T=20°C; 1 h;
参考文献
Manabe, Shino; Ueki, Akiharu; Ito, Yukishige
Tetrahedron Letters, 2008 , vol. 49, # 35 p. 5159 - 5161
反应条件
methanol; sodium methylate T=20°C; 1.5 h;
参考文献
Pinto, Tiago A.D.; Hrdina, Radim; Kirsch, Gilbert; Oliveira-Campos, Ana M.F.; Rodrigues, Ligia M.; Esteves, Ana P.
Arkivoc, 2012 , vol. 2012, # 6 p. 185 - 193
反应条件
1: With polystyrene-bound [1,3,2]diazaphosphorinane in dichloromethane T=20°C; 0.166667 h; 2: With potassium hydroxide in methanol T=60°C; 3 h;
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 11 p. 1672 - 1676
反应条件
1: With AgroPore(R); N-ethyl-N,N-diisopropylamine in dichloromethane; N,N-dimethyl-formamide T=20°C; 12 h; 2: With trifluoroacetic acid in methanol; dichloromethane T=20°C; 0.25 h;
参考文献
Tanaka, Hiroshi; Ishida, Tadasuke; Matoba, Nobuatsu; Tsukamoto, Hirokazu; Yamada, Haruo; Takahashi, Takashi
Angewandte Chemie - International Edition, 2006 , vol. 45, # 38 p. 6349 - 6352
反应条件
water in acetonitrile 0.583333 h; UV-irradiation;
参考文献
Wang, Pengfei; Zhou, Lei; Zhang, Xin; Liang, Xing
Chemical Communications, 2010 , vol. 46, # 9 p. 1514 - 1516
