1-(2氯乙氧基)-2-(2-甲氧基乙氧基)乙烷合成路线 （共 12 条）
反应条件
1: 1) sodium / 1) 100-120 deg C, 2) 100-120 deg C, 2-3 h 2: 51 percent / potassium hydroxide, potassium permanganate / H2O / 12 h / Ambient temperature View Scheme
参考文献
Heimann, Ulrich; Voegtle, Fritz
Liebigs Annalen der Chemie, 1980 , # 6 p. 858 - 862
反应条件
sodium 1) 100-120 deg C, 2) 100-120 deg C, 2-3 h; Yield given. Multistep reaction;
参考文献
Norrman; Papra; Kamounah; Gadegaard; Larsen
Journal of Mass Spectrometry, 2002 , vol. 37, # 7 p. 699 - 708
反应条件
in N,N-dimethyl-formamide 10 h; Reflux;
参考文献
Yerramreddy, Thirupathi Reddy; Milewski, Mikolaj; Penthala, Narsimha Reddy; Stinchcomb, Audra L.; Crooks, Peter A.
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 11 p. 3280 - 3283
参考文献
Yanagida,S. et al.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 3111 - 3120
参考文献
Yanagida,S. et al.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 3111 - 3120
反应条件
(i) NaH, 1,2-dimethoxyethane, (ii) /BRN= 1700211/; Multistep reaction;
参考文献
Chaput,G. et al.
Canadian Journal of Chemistry, 1975 , vol. 53, p. 2240 - 2246
反应条件
pyridine; thionyl chloride in chloroform
3 h; Heating;
参考文献
Gudipati, Venugopal; Curran, Dennis P.; Wilcox, Craig S.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3599 - 3607
反应条件
(i) BF3-Et2O, (ii) SOCl2; Multistep reaction;
参考文献
Gerhardt,W.; Kucharski,S.
Journal fuer Praktische Chemie (Leipzig), 1977 , vol. 319, p. 705 - 712
反应条件
(i) NaH, 1,2-dimethoxyethane, (ii) /BRN= 1700211/; Multistep reaction;
参考文献
Chaput,G. et al.
Canadian Journal of Chemistry, 1975 , vol. 53, p. 2240 - 2246
反应条件
sodium azide; tetrabutyl-ammonium chloride in water
8 h; Heating;
参考文献
Hawker, Craig J.; Saville, Paul M.; White, John W.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3503 - 3505
