4’-甲氧基联苯-4-甲醛合成路线 (共 36 条)
反应条件
pyridine; lead(IV) acetate
参考文献
Analytical Chemistry, , vol. 52, # 14 p. 2417 - 2420
反应条件
potassium carbonate; 2-(dicyclohexylphosphino)-2'-methylbiphenyl; palladium on activated charcoal in N,N-dimethyl acetamide; water T=80°C; Suzuki-Miyaura cross-coupling; 24 h;
参考文献
Tetrahedron, , vol. 63, # 51 p. 12646 - 12654
反应条件
NiCl2(PCy3)2 in benzene T=25°C; 1 h;
参考文献
Organometallics, , vol. 30, # 6 p. 1299 - 1302
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium chloride in ethanol; toluene Suzuki coupling; Heating;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 13 p. 1709 - 1712
反应条件
palladium diacetate T=100°C; Stille cross-coupling; 15 h; Ionic liquid;
参考文献
European Journal of Organic Chemistry, , # 1 p. 143 - 149
反应条件
1: MnCl2 / tetrahydrofuran / 24 h / 20 °C 2: SiO2 / CH2Cl2; pentane View Scheme
参考文献
Synthesis, , # 12 p. 2138 - 2144
反应条件
1: With toluene-4-sulfonic acid in benzene 3 h; Reflux; 2: With chromium(VI) oxide; acetic acid in water T=10 - 20°C; 23 h;
参考文献
Helvetica Chimica Acta, , vol. 91, # 3 p. 559 - 568
反应条件
potassium carbonate in ethanol; water T=50°C; Suzuki coupling; 20 h;
参考文献
European Journal of Organic Chemistry, , # 13 p. 2635 - 2642
反应条件
1: para-iodoanisole With copper; zinc in N,N-dimethyl-formamide T=125°C; 0.25 h; 2: 4-bromo-benzaldehyde With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=100°C; Negishi cross-coupling reaction; 0.25 h; Further stages.;
参考文献
Tetrahedron Letters, , vol. 45, # 20 p. 3909 - 3912
反应条件
2-Nitropropane; sodium ethanolate
参考文献
Journal of the American Chemical Society, , vol. 96, # 14 p. 4611 - 4616