4’-甲氧基联苯-4-甲醛合成路线 （共 36 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; copper(l) iodide; triphenylphosphine in water; N,N-dimethyl-formamide T=100°C; Suzuki-Miyaura cross-coupling; 1 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 52, # 10 p. 1132 - 1135
反应条件
sodium carbonate in ethanol T=75°C; Suzuki-Miyaura cross coupling; 2 h;
参考文献
Journal of Chemical Research, , vol. 35, # 4 p. 246 - 250
反应条件
1: With diisobutylaluminium hydride in dichloromethane T=0 - 20°C; 19 h; 2: With hydrogenchloride; water in dichloromethane T=20°C;
参考文献
WO2005/30702 A1, ;
Page/Page column 47 ;
反应条件
potassium hydroxide in tetrahydrofuran; water T=60°C; Suzuki-Miyaura Coupling; 0.0833333 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 18 p. 3456 - 3460
反应条件
potassium carbonate in ethanol; water T=50°C; Suzuki-Miyaura Coupling; 19 h; Reagent/catalyst;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 10 p. 2007 - 2018
反应条件
KF in tetrahydrofuran
反应条件
sodium 2-(2-pyridin-3-ylethylamino)ethyl sulfonate; palladium dichloride in water T=20°C; Suzuki coupling; 3 h;
参考文献
Tetrahedron Letters, , vol. 49, # 41 p. 5858 - 5862
反应条件
1: p-methoxy-phenylmagnesium chloride With N,N,N',N,-tetramethylethylenediamine; zinc(II) chloride in tetrahydrofuran T=80°C; 0.25 h; microwave irradiation; 2: 4-bromo-benzaldehyde With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; Negishi cross-coupling; 0.0833333 h;
参考文献
Tetrahedron, , vol. 61, # 47 p. 11168 - 11176
反应条件
sodium carbonate; palladium on activated charcoal in ethanol; water T=20°C; Suzuki-Miyaura cross-coupling; 24 h;
参考文献
Tetrahedron, , vol. 63, # 43 p. 10596 - 10602
反应条件
1: 4-methoxyphenyl magnesium bromide With N,N,N',N,-tetramethylethylenediamine; zinc(II) chloride in tetrahydrofuran T=80°C; 0.25 h; microwave irradiation; 2: 4-bromo-benzaldehyde With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; Negishi cross-coupling; 0.0833333 h;
参考文献
Tetrahedron, , vol. 61, # 47 p. 11168 - 11176
