2-硝基对苯二甲酸二甲酯合成路线 （共 23 条）
反应条件
potassium hydroxide; sodium hydroxide in methanol; water; N,N-dimethyl-formamide
参考文献
Ciba-Geigy Corporation
Patent: US4348530 A1, 1982 ;
反应条件
1: dimethylformamide / -30 °C
2: 1.) KOH, 2.) H+
3: polyphosphoric acid / 160 °C
View Scheme
参考文献
Breslow, Ronald; Guo, Tao
Tetrahedron Letters, 1987 , vol. 28, # 28 p. 3187 - 3188
反应条件
1.1: sodium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C
1.2: 1.5 h / 75 °C
2.1: chlorosulfonic acid / 1 h / 5 - 10 °C
View Scheme
参考文献
LAMBERTI SPA; CASIRAGHI, Angelo; MENEGUZZO, Enzo; NORCINI, Gabriele; BELLOTTI, Elena; FLORIDI, Giovanni; LI BASSI, Giuseppe
Patent: WO2012/62692 A1, 2012 ;
