1,2,3,4-四氢-1-萘酚合成路线 （共 211 条）
反应条件
1: 34 percent / n-BuLi; TMEDA / pentane; hexane / -78 - 20 °C 2: 41 percent / CrO3; AcOH / H2O / 12 h / 20 °C View Scheme
参考文献
Lebedev, Artyom Y.; Khartulyari, Anton S.; Voskoboynikov, Alexander Z.
Journal of Organic Chemistry, 2005 , vol. 70, # 2 p. 596 - 602
反应条件
Lawesson's reagent in toluene 0.5 h; Heating;
参考文献
Nishio, Takehiko
Journal of the Chemical Society, Chemical Communications, 1989 , # 4 p. 205 - 206
反应条件
1: Et3N; DMAP / CH2Cl2 2: 64 percent / KMnO4; MgSO4*7H2O / acetone; H2O / 5 h View Scheme
参考文献
Joly; Nair, Mangalam S.
Tetrahedron Asymmetry, 2001 , vol. 12, # 16 p. 2283 - 2287
反应条件
1: 93 percent / oxalic acid / H2O / 6 h / Heating 2: 1.) formic acid, 30 percent hydrogen peroxide; 2.) 20 percent H2SO4 / 1.) 35 deg C, 2 h, room temp., 12 h; 2.) reflux, 10 h 3: 93 percent / NaH / benzene / 5 h / 65 - 70 °C View Scheme
参考文献
Vebrel, Joel; Carrie, Robert
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 5-6 p. 161 - 166
反应条件
1: 65.4 percent / conc. HCl / acetic acid / 1.17 h / Heating 2: 72.4 percent / Br2 / CCl4 / 0.5 h / 0 °C 3: 54 percent / piperidine / benzene View Scheme
参考文献
Radhakrishna, A. S.; Berlin, K. Darrell; Helm, Dick van der
Polish Journal of Chemistry, 1980 , vol. 54, # 3 p. 495 - 502
反应条件
1.1: triethylamine / dichloromethane / 0.42 h / 0 °C / Inert atmosphere 2.1: sodium azide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere 3.1: boron trifluoride diethyl etherate / dichloromethane / -78 - 20 °C / Inert atmosphere 3.2: 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Murali, Annamalai; Puppala, Manohar; Varghese, Babu; Baskaran, Sundarababu
European Journal of Organic Chemistry, 2011 , # 27 p. 5297 - 5302
反应条件
N,N-dichloro-p-toluenesulphonamide in acetonitrile T=40°C; 1.5 h;
参考文献
Kim, Yong Hae; Lee, In Sang; Lim, Sang Chul
Chemistry Letters, 1990 , # 7 p. 1125 - 1128
反应条件
1: 2-methyl-butan-2-ol / Heating 2: Pd-C / 180 °C 3: <Me3O>BF4 / CH2Cl2 View Scheme
参考文献
Felix,D. et al.
Helvetica Chimica Acta, 1969 , vol. 52, p. 1030 - 1042
参考文献
Hendrickson,J.B.; Joffee,I.
Journal of the American Chemical Society, 1973 , vol. 95, p. 4083 - 4084
反应条件
1: Et3N; DMAP / CH2Cl2 2: 64 percent / KMnO4; MgSO4*7H2O / acetone; H2O / 5 h 3: 94 percent / aq. K2CO3 / methanol / 0.25 h / 30 °C View Scheme
参考文献
Joly; Nair, Mangalam S.
Tetrahedron Asymmetry, 2001 , vol. 12, # 16 p. 2283 - 2287
