反应条件
1: 67 percent / LiAlH4 / tetrahydrofuran / 10 h / Heating 2: 87 percent / Zn / acetic acid / 4 h / 50 - 60 °C 3: 90 percent / H2 / 5percent Pd on charcoal / methanol / 16 h 4: 1.) SOCl2, 2.) TABD / 1.) CDCl3, 0 deg C to room temperature, 19.5 h, 2.) 12 h View Scheme
参考文献
Tetrahedron, , vol. 54, # 36 p. 10899 - 10914
