反应条件
1: 68 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene / 1,2-dimethoxy-ethane / 0 °C
2: p-toluenesulfonic acid / Ambient temperature
3: 82 percent / lithium iodide hydrate / dimethylformamide / 4 h / Heating
4: 84 percent / NaH / 1,2-dimethoxy-ethane / 4 h / Ambient temperature
5: LiAlH4 / diethyl ether / 1 h / 0 °C
6: 19 percent / Se / 3 h / 300 °C
View Scheme
参考文献
Harre, Michael; Winterfeldt, Ekkehard
Chemische Berichte, 1982 , vol. 115, # 4 p. 1437 - 1447