2,4,5-三甲基苯甲酸合成路线 （共 28 条）
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate in acetic acid T=25°C; P=760 Torr; 12 h;
参考文献
Yoshino, Yasushi; Hayashi, Yoshiaki; Iwahama, Takahiro; Sakaguchi, Satoshi; Ishii, Yasutaka
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 6810 - 6813
反应条件
oxygen; zirconium (IV) sulphate; anhydrous cobalt diacetate; Manganese (II) acetate; 2,6-dihydroxypyromellitimide in acetic acid T=60 - 70°C; P=6000.6 Torr; 2 h; Product distribution / selectivity;
参考文献
US2011/71314 A1, ;
Page/Page column 13-14 ;
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate in acetic acid T=25°C; P=760 Torr; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 62, # 20 p. 6810 - 6813
反应条件
carbon dioxide in tetrahydrofuran
参考文献
US6162808 A1, ;
US 6162808 A
反应条件
nitrogen(IV) oxide in various solvent(s) T=20°C; 0.5 h; in the dark; Title compound not separated from byproducts;
参考文献
Acta Chemica Scandinavica, , vol. 50, # 11 p. 991 - 1008
反应条件
2-hydroxy-1,3-isoindolinedione; xanthone powder; oxygen; anhydrous tetramethylammonium chloride in acetonitrile T=60°C; P=3750.38 Torr; 3 h; Autoclave;
参考文献
Tetrahedron Letters, , vol. 50, # 15 p. 1677 - 1680
反应条件
water; oxygen; bromide; anhydrous cobalt diacetate; Manganese (II) acetate in acetic acid T=95°C; atmospheric pressure; Further byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 2-3 p. 297 - 306
反应条件
1: propynecarboxylic acid With 2-bromobenzene boronic acid in 1,2-dichloro-ethane T=50°C; 0.166667 h; Inert atmosphere; 2: 2,3-dimethyl-buta-1,3-diene in 1,2-dichloro-ethane T=50°C; Diels-Alder cycloaddition; 96 h; Inert atmosphere; 3: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,2-dichloro-ethane T=25°C; 4 h; Inert atmosphere;
参考文献
Zheng, Hongchao; Hall, Dennis G.
Tetrahedron Letters, 2010 , vol. 51, # 27 p. 3561 - 3564
反应条件
Keggin Mo catalyst; nitric acid T=80°C;
参考文献
Journal of the American Chemical Society, , vol. 126, # 20 p. 6356 - 6362
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=25°C; 4 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 51, # 27 p. 3561 - 3564
