2-氧代-1-环庚烷甲酸甲酯合成路线 （共 17 条）
反应条件
1: With sodium hydride in mineral oil; benzene 3.84 h; Inert atmosphereReflux; 2: With acetic acid in mineral oil; benzene T=0°C; Inert atmosphere;
参考文献
Ikeda, Shuhei; Shibuya, Masatoshi; Kanoh, Naoki; Iwabuchi, Yoshiharu
Organic Letters, 2009 , vol. 11, # 8 p. 1833 - 1836
反应条件
n-butyllithium; diisopropylamine 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C to 25 deg C, 3 h; Multistep reaction;
参考文献
Winkler, Jeffrey D.; Hong, Bor-Cherng; Hey, John P.; Williard, Paul G.
Journal of the American Chemical Society, 1991 , vol. 113, # 23 p. 8839 - 8846
反应条件
methanol; sodium Heating;
参考文献
Sum,P.-E.; Weiler,L.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 996 - 1000
反应条件
1: aq. NaOH, <PhCH2NEt3>Cl 2: Fe(NO3)3 / (electrolysis) View Scheme
参考文献
Torii,S. et al.
Journal of the Chemical Society, Chemical Communications, 1978 , p. 293 - 294
反应条件
1: (i) NaH, THF, (ii) nBuLi, hexane, (iii) /BRN= 1071199/ 2: Na, MeOH / Heating View Scheme
参考文献
Sum,P.-E.; Weiler,L.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 996 - 1000
反应条件
iron nitrate (III) (electrolysis);
参考文献
Torii,S. et al.
Journal of the Chemical Society, Chemical Communications, 1978 , p. 293 - 294
反应条件
(Et3NH)3PO4 1.) DMF, electrochemical reduction; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carelli, Italo; Curulli, Antonella; Inesi, Achille; Zeuli, Errico
Journal of Chemical Research, Miniprint, 1990 , # 3 p. 620 - 644
反应条件
metastable ion fragmentation reaction of selected ions;
参考文献
Harrison, Alex. G.; Kallury, R. Krishna Mohan Rao; Krull, Ulrich J.; Thompson, Michael
Organic Mass Spectrometry, 1988 , vol. 23, p. 723 - 728
反应条件
iron(III) chloride 1 h; Ambient temperature;
参考文献
Christoffers, Jens
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 21 p. 3141 - 3149
反应条件
1.1: 22 percent / aq. HCl; molecular sieves 4 Angstroem / toluene / 60 - 65 °C 2.1: Cu(OAc)2*H2O / acetone / 1 h / 23 °C 2.2: acetone / 23 °C 2.3: 75 percent / aq. HCl / 0 °C View Scheme
参考文献
Christoffers, Jens; Mann, Alexander
Chemistry - A European Journal, 2001 , vol. 7, # 5 p. 1014 - 1027
