4-乙酰氧基-2-溴-5-甲氧基苯甲醛合成路线 （共 5 条）
反应条件
bromine; potassium bromide in water T=0 - 20°C; 15 h;
参考文献
Takaya, Daisuke; Yamashita, Atsuya; Kamijo, Kazue; Gomi, Junko; Ito, Masahiko; Maekawa, Shinya; Enomoto, Nobuyuki; Sakamoto, Naoya; Watanabe, Yoshiaki; Arai, Ryoichi; Umeyama, Hideaki; Honma, Teruki; Matsumoto, Takehisa; Yokoyama, Shigeyuki
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 22 p. 6892 - 6905
反应条件
1: pyridine / dichloromethane / 18 h / 20 °C 2: bromine; potassium bromide / water / 15 h / 0 - 20 °C View Scheme
参考文献
Chen, Han; Long, Haitao; Cui, Xiaojie; Zhou, Jiang; Xu, Ming; Yuan, Gu
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2583 - 2591
反应条件
hydrogenchloride; water T=90°C; 4 h;
参考文献
Takaya, Daisuke; Yamashita, Atsuya; Kamijo, Kazue; Gomi, Junko; Ito, Masahiko; Maekawa, Shinya; Enomoto, Nobuyuki; Sakamoto, Naoya; Watanabe, Yoshiaki; Arai, Ryoichi; Umeyama, Hideaki; Honma, Teruki; Matsumoto, Takehisa; Yokoyama, Shigeyuki
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 22 p. 6892 - 6905
反应条件
1: 88 percent / KOH / tetrahydrofuran; H2O / 2 h / Ambient temperature
2: 98 percent / dimethylformamide / 3 h / 80 °C
View Scheme
参考文献
Chen, Han; Long, Haitao; Cui, Xiaojie; Zhou, Jiang; Xu, Ming; Yuan, Gu
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2583 - 2591
反应条件
sodium hydroxide; sodium tetrahydroborate
参考文献
Anhoury; Crooy; De Neys; Eliaers
Bulletin des Societes Chimiques Belges, 1974 , vol. 83, # 3-4 p. 117 - 124
