4-(9-咔唑)基-4苯胺合成路线 (共 13 条)
反应条件
1: pyridine / dichloromethane / 3 h / 0 °C / |Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; potassium phosphate / toluene / 5 h / 100 °C / |Inert atmosphere
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参考文献
Hung, Tran Quang; Thang, Ngo Ngoc; Hoang, Do Huy; Dang, Tuan Thanh; Villinger, Alexander; Langer, Peter
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 16 p. 2596 - 2605
反应条件
1: cesium fluoride / dimethyl sulfoxide / 15 h / 150 °C
2: 10 palladium on activated charcoal; hydrazine hydrate / ethanol / 6 h / Reflux
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参考文献
Chiu, Ssu-Kai; Chung, Yi-Chun; Liou, Guey-Sheng; Su, Yuhlong Oliver
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 3 p. 331 - 337
反应条件
1: potassium carbonate
2: aqueous hydrochloric acid; tin
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参考文献
Nelmes; Tucker
Journal of the Chemical Society, 1933 , p. 1523