4-[(E)-(羟基亚胺)甲基]苯甲腈合成路线 （共 9 条）
反应条件
[Ru(κ(3)-tpy)(κ(1)-P-PPh2Py)Cl2] in toluene Beckmann rearrangement; 12 h; Reflux;
参考文献
Kumar, Prashant; Singh, Ashish Kumar; Pandey, Rampal; Pandey, Daya Shankar
Journal of Organometallic Chemistry, 2011 , vol. 696, # 22 p. 3454 - 3464
反应条件
10 CuO-ZnO on activated carbon in toluene T=100°C; 4 h; Inert atmosphere;
参考文献
Sharma, Sumeet K.; Bishopp, Simon D.; Liana Allen; Lawrence, Ruth; Bamford, Mark J.; Lapkin, Alexei A.; Plucinski, Pawel; Watson, Robert J.; Williams, Jonathan M.J.
Tetrahedron Letters, 2011 , vol. 52, # 33 p. 4252 - 4255
反应条件
methanesulfonic acid; zinc in acetonitrile T=25°C; reduction;
参考文献
Kise, Naoki; Ueda, Nasuo
Tetrahedron Letters, 2001 , vol. 42, # 12 p. 2365 - 2368
反应条件
10 CuO-ZnO on activated carbon in toluene T=100°C; 4 h; Inert atmosphere;
参考文献
Sharma, Sumeet K.; Bishopp, Simon D.; Liana Allen; Lawrence, Ruth; Bamford, Mark J.; Lapkin, Alexei A.; Plucinski, Pawel; Watson, Robert J.; Williams, Jonathan M.J.
Tetrahedron Letters, 2011 , vol. 52, # 33 p. 4252 - 4255
反应条件
potassium fluoride on basic alumina in N,N-dimethyl-formamide T=85°C; 2 h;
参考文献
Movassagh, Barahman; Shokri, Salman
Synthetic Communications, 2005 , vol. 35, # 6 p. 887 - 890
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile 0.5 h; Photolysis; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 71, # 20 p. 7785 - 7792
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in tetrahydrofuran; dimethyl sulfoxide 0.333333 h; Ambient temperature;
参考文献
Bose, D. Subhas; Srinivas
Synlett, 1998 , # 9 p. 977 - 978
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile 0.5 h; Photolysis; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 71, # 20 p. 7785 - 7792
反应条件
1: Cl2(gas) / CHCl3
2: 92 percent
View Scheme
参考文献
Kumagai, T.; Shimizu, K.; Kawamura, Y.; Mukai, T.
Tetrahedron, 1981 , vol. 37, # 19 p. 3365 - 3376
