2,6-二甲基-2,5-环己二烯-1,4-二酮合成路线 （共 148 条）
反应条件
[bis(acetoxy)iodo]benzene T=20°C; Oxidation; cyclization; 1 h;
参考文献
Camps, Pelayo; Gonzalez, Albert; Munoz-Torrero, Diego; Simon, Montserrat; Zuniga, Adriana; Martins, Miriam A.; Font-Bardia, Merce; Solans, Xavier
Tetrahedron, 2000 , vol. 56, # 41 p. 8141 - 8151
反应条件
1: 76 percent / tetrahydrofuran; diethyl ether / 3 h / -78 - 20 °C 2: 6 percent / PCC; SiO2 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Kim, Hee Jin; Koo, Sangho
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 19 p. 3479 - 3481
反应条件
1: 81 percent / toluene / 4 h / Heating 2: 76 percent / tetrahydrofuran; diethyl ether / 3 h / -78 - 20 °C 3: 6 percent / PCC; SiO2 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Kim, Hee Jin; Koo, Sangho
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 19 p. 3479 - 3481
参考文献
Bushmelev; Genaev; Shubin
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 1 p. 62 - 66
反应条件
water in acetone 5 h; Heating;
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
反应条件
sulfuric acid; nitric acid in nitromethane T=2°C; 1 h; Product distribution;
参考文献
Tashiro, Masashi; Yamato, Takehiko; Fukata, Gouki; Fukuda, Yasuhisa
Journal of Organic Chemistry, 1981 , vol. 46, # 11 p. 2376 - 2379
反应条件
1: Sn, HCl 2: 2.) reflux 3: 51.6 percent HNO3 / nitrous acid / 1 h / 0 °C View Scheme
参考文献
Helsby, Paul; Ridd, John H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 311 - 316
反应条件
1: 2.) reflux 2: 51.6 percent HNO3 / nitrous acid / 1 h / 0 °C View Scheme
参考文献
Helsby, Paul; Ridd, John H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 311 - 316
反应条件
2-methyl-propan-1-ol; water T=20°C; 1461 h;
参考文献
Avdeenko; Konovalova; Mikhailichenko; Santalova; Palamarchuk; Shishkin
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 5 p. 642 - 650
反应条件
sulfuric acid; dichromate(VI)(2-)
参考文献
Nallaiah, C.; Strickson, J. A.
Tetrahedron, 1986 , vol. 42, # 14 p. 4083 - 4088
