2,6-二甲基-2,5-环己二烯-1,4-二酮合成路线 (共 148 条)
反应条件
oxygen; acetone-oxime in various solvent(s) T=40°C; P=860.3 Torr; 6 h;
参考文献
Takehira, Katsuomi; Shimizu, Masao; Watanabe, Yoshihito; Orita, Hideo; Hayakawa, Takashi
Tetrahedron Letters, 1990 , vol. 31, # 18 p. 2607 - 2608
反应条件
water in acetone 6 h; Heating;
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
反应条件
Mn(1-nnap)2; oxygen; triphenylphosphine in dichloromethane T=50°C; Oxidation; dimerization; P=15200 Torr; 3 h;
参考文献
Srivastava, Sumit; Ali, Afsar; Tyagi, Adish; Gupta, Rajeev
European Journal of Inorganic Chemistry, 2014 , # 12 p. 2113 - 2123
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; 1,3-dimethyl-5-ethyl-4a-hydroperoxyalloxazine; oxygen; sodium hydrogencarbonate in water; acetonitrile T=20°C; Dakin Phenol Oxidation; 3 h;
参考文献
Chen, Shuai; Foss, Frank W.
Organic Letters, 2012 , vol. 14, # 19 p. 5150 - 5153,4
反应条件
sulfuric acid in ethylene glycol dimethyl ether Hydrolysis; 1 h; Heating;
参考文献
Omura, Kanji
Synthetic Communications, 2000 , vol. 30, # 5 p. 877 - 885
反应条件
sulfuric acid; sodium nitrite T=20°C; 0.333333 h;
参考文献
Bucher, Goetz; Sander, Wolfram
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1346 - 1351
反应条件
1: m-chloroperoxybenzoic acid / CH2Cl2 / 2 h / 0 °C 2: 34 percent / 2,6-dimethylphenol, potassium tert-butoxide, 18-crown-6 / 2-methyl-propan-2-ol / 72 h / 25 °C View Scheme
参考文献
Wagner, William R.; Spero, Denice M.; Rastetter, William H.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1476 - 1480
反应条件
oxygen; Co(3,5-Br2-SMDPT) in toluene P=3878.6 Torr; 24 h; Ambient temperaturesev. cobalt dioxygen complexes with derivatized tetra- and pentadentane Schiff-base ligands and influence of the latter one's steric and electronic effects discussed; var. time; KineticsMechanismProduct distribution;
参考文献
Corden, Barry B.; Drago, Russel S.; Perito, Richard P.
Journal of the American Chemical Society, 1985 , vol. 107, # 10 p. 2903 - 2907
反应条件
perchloric acid; ceric perchlorate in acetonitrile T=24.9°C;
参考文献
Leszczynski, L.; Dziegiec, J.
Polish Journal of Chemistry, 1994 , vol. 68, # 9 p. 1855 - 1862
反应条件
Ni0.64Al0.36(OH)2[WO4(2-)0.045NO3(1-)0.27]*0.6H2O; dihydrogen peroxide; NH4Br in tetrahydrofuran; water
参考文献
Sels; De Vos; Jacobs
Angewandte Chemie - International Edition, 2005 , vol. 44, # 2 p. 310 - 313