titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate in dichloromethane; water; toluene
T=-50°C; 72 h; Yield given. Title compound not separated from byproducts;
参考文献
Boussad, N.; Trefouel, T.; Dupas, G.; Bourguignon, J.; Queguiner, G.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 66, # 1.4 p. 127 - 138
1: dimethylformamide / 24 h / 80 °C
2: Ti(OiPr)4, (R,R)-Diethyl tartrate, tBuOOH / CH2Cl2; H2O; toluene / Ambient temperature
View Scheme
参考文献
Boussad, N.; Trefouel, T.; Dupas, G.; Bourguignon, J.; Queguiner, G.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 66, # 1.4 p. 127 - 138
Boussad, N.; Trefouel, T.; Dupas, G.; Bourguignon, J.; Queguiner, G.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 66, # 1.4 p. 127 - 138