2,5-二氮杂环丙烷基-1,4-苯醌合成路线 (共 17 条)
反应条件
nickel; ethyl acetate Hydrogenation;
参考文献
Marxer
Helvetica Chimica Acta, 1955 , vol. 38, p. 1473,1487
Helvetica Chimica Acta, 1956 , vol. 39, p. 335,339
参考文献
Makarowa; Berlin
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 666,667,668,670
engl.Ausg., vol. 659, p. 660,661,662
参考文献
Makarowa; Berlin
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 666,667,668,670
engl.Ausg., vol. 659, p. 660,661,662
反应条件
in N,N-dimethyl acetamide; water T=40°C; 24 h; product yield/distribution; mechanism; apparent activation energy; 0.01 M phosphate buffer (pH 8); examination of pH (further buffers), ionic strength, buffer concentration and reaction time; Rate constantKineticsThermodynamic data;
参考文献
Kusai; Tanaka; Ueda
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 12 p. 3671 - 3679
反应条件
sodium methylate in chloroform T=60°C; 2 h;
参考文献
Kusai; Tanaka; Ueda
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 7 p. 2983 - 2989
反应条件
in N,N-dimethyl acetamide T=60°C; degradation in various solvents; MechanismProduct distributionRate constant;
参考文献
Kusai; Tanaka; Ueda
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 7 p. 2983 - 2989
参考文献
Makarowa; Berlin
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 666,667,668,670
engl.Ausg., vol. 659, p. 660,661,662
参考文献
Makarowa; Berlin
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 666,667,668,670
engl.Ausg., vol. 659, p. 660,661,662
反应条件
in N,N-dimethyl acetamide; water
T=40°C; 24 h; product yield/distribution; mechanism; apparent activation energy; 0.01 M phosphate buffer (pH 8); examination of pH (further buffers), ionic strength, buffer concentration and reaction time; Rate constantKineticsThermodynamic data;
参考文献
Kusai; Tanaka; Ueda
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 12 p. 3671 - 3679
参考文献
Farbenfabr. Bayer
Patent: DE967794 , 1954 ;
Full Text Show Details
Petersen et al.
Angewandte Chemie, 1955 , vol. 67, p. 217,219