2,3-二甲基-5-氟吲哚合成路线 （共 3 条）
反应条件
in acetic acid T=120°C; 2 h;
参考文献
Lopez-Iglesias, Maria; Busto, Eduardo; Gotor, Vicente; Gotor-Fernandez, Vicente
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8049 - 8055,7
Title/Abstract Full Text Show Details
Lopez-Iglesias, Maria; Busto, Eduardo; Gotor, Vicente; Gotor-Fernandez, Vicente
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8049 - 8055
反应条件
1: sec.-butyllithium With zinc dibromide in tetrahydrofuran T=0°C; 0.166667 h; Inert atmosphere; 2: With zinc dibromide in tetrahydrofuran T=25°C; 0.166667 h; Inert atmosphere; 3: 4-fluorobenzenediazonium tetrafluoroborate With chloro-trimethyl-silane in tetrahydrofuran T=-60 - 125°C; Inert atmosphereMicrowave irradiation; regioselective reaction;
参考文献
Zhang, Zhi-Guang; Haag, Benjamin A.; Li, Jin-Shan; Knochel, Paul
Synthesis, 2011 , # 1 p. 23 - 29
反应条件
RuCl3*xH2O; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene T=110 - 170°C; 25 h;
参考文献
Tursky, Matyas; Lorentz-Petersen, Linda L. R.; Olsen, Lasse B.; Madsen, Robert
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 24 p. 5576 - 5582
