4-甲基-3-环己烯-1-酮合成路线 （共 33 条）
反应条件
hydrogenchloride in ethyl acetate
参考文献
SmithKline Beechman Corp.
Patent: US5438118 A1, 1995 ;
US 5438118 A
反应条件
ammonia; lithium in tetrahydrofuran; ethanol 0.333333 h;
参考文献
Nishimura, Hiroyuki; Takabatake, Tetsuhiko; Kaku, Koichiro; Seo, Akira; Mizutani, Junya
Agricultural and Biological Chemistry, 1981 , vol. 45, # 8 p. 1861 - 1864
反应条件
boron trifluoride diethyl etherate in dichloromethane T=0°C; 2 h;
参考文献
Smith,A.B.; Toder,B.H.; Branca,S.J.
Journal of the American Chemical Society, 1981 , vol. 103, p. 1996
反应条件
oxalic acid in diethyl ether T=20°C; 1.5 h;
参考文献
Parladar, Vesile; Gueltekin, M. Serdar; Celik, Murat
Journal of Chemical Research, 2006 , # 1 p. 10 - 11
反应条件
silver nitrate in tetrahydrofuran; diethyl ether; water T=20°C; 1 h;
参考文献
Boucher, Jean-Luc; Stella, Lucien
Tetrahedron, 1985 , vol. 41, # 5 p. 875 - 887
反应条件
sodium periodate in methanol; water
参考文献
Sasaki, Tadashi; Ishibashi, Yukio; Ohno, Masatomi
Tetrahedron Letters, 1982 , vol. 23, # 16 p. 1693 - 1696
反应条件
1: 84 percent / Jones reagent / acetone / 1 h / 0 °C 2: SOCl2 / 4 h 3: diethyl ether 4: 55 percent / boron trifluoride etherate / CH2Cl2 / 2 h / 0 °C View Scheme
参考文献
Smith,A.B.; Toder,B.H.; Branca,S.J.
Journal of the American Chemical Society, 1981 , vol. 103, p. 1996
反应条件
1: SOCl2 / 4 h 2: diethyl ether 3: 55 percent / boron trifluoride etherate / CH2Cl2 / 2 h / 0 °C View Scheme
参考文献
Smith,A.B.; Toder,B.H.; Branca,S.J.
Journal of the American Chemical Society, 1981 , vol. 103, p. 1996
反应条件
1: diethyl ether 2: 55 percent / boron trifluoride etherate / CH2Cl2 / 2 h / 0 °C View Scheme
参考文献
Smith,A.B.; Toder,B.H.; Branca,S.J.
Journal of the American Chemical Society, 1981 , vol. 103, p. 1996
反应条件
nitromethane; zinc dibromide in dichloromethane 4 h; Ambient temperature;
参考文献
Bhushan, Vidya; Rajopadhye, M. M.; Chandrasekaran, S
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 424 - 425
