反应条件
1: 1.) Mg / 1.) Et2O, reflux, 30 min 2.) THF, rt, overnight
2: 81 percent / H2 / 10percent Pd/C / ethanol
3: 11 percent / borate buffer pH 9, potassium nitrosodisulfonate (Fremy-salt) / ethanol; H2O / 5 h
View Scheme
参考文献
Koenig, Wilfried A.; Faasch, Holger; Heitsch, Holger; Colberg, Cornelia; Hausen, Bjoern M.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1993 , vol. 48, # 3 p. 387 - 393
