1,-脱水-3,-O-异丙二烯-β-D-谷氨酸五乙酸酯合成路线 (共 9 条)
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide 1 h; Ambient temperature;
参考文献
Sarbajna, Sumita; Roy, Nirmolendu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 3 p. 252 - 256
反应条件
copper(II) sulfate; acetone
参考文献
Micheel
Chemische Berichte, 1929 , vol. 62, p. 687,692
Full Text Show Details
Hann; Hudson
Journal of the American Chemical Society, 1942 , vol. 64, p. 2435,2436
反应条件
sulfuric acid; acetone Erhitzen des Reaktionsprodukts unter vermindertem Druck;
参考文献
McCreath; Smith
Journal of the Chemical Society, 1939 , p. 387,389
反应条件
toluene-4-sulfonic acid
参考文献
Abdel-Rahman; Adams; Boyes; Kelly; Mansfield; Procoplou; Roberts; Slee; Watson
Journal of the Chemical Society - Series Chemical Communications, 1993 , # 24 p. 1839 - 1841
参考文献
Micheel
Chemische Berichte, 1929 , vol. 62, p. 687,692
Full Text Show Details
Hann; Hudson
Journal of the American Chemical Society, 1942 , vol. 64, p. 2435,2436
反应条件
1: 95 percent / NaH; tetrabutylammonium iodide / dimethylformamide / 20 °C 2: 80 percent / trifluoroacetic acid / 0 - 20 °C View Scheme
参考文献
Goff, Randal D.; Gao, Ying; Mattner, Jochen; Zhou, Dapeng; Yin, Ning; Cantu III, Carlos; Teyton, Luc; Bendelac, Albert; Savage, Paul B.
Journal of the American Chemical Society, 2004 , vol. 126, # 42 p. 13602 - 13603
参考文献
Hann; Hudson
Journal of the American Chemical Society, 1942 , vol. 64, p. 2435,2436
反应条件
1: 89 percent / pyridine / 3 h / Ambient temperature
2: 77 percent / aq. H2SO4 / dioxane / 16 h / 80 °C
View Scheme
参考文献
Paulsen, Hans; Schnell, Dagmar
Chemische Berichte, 1981 , vol. 114, # 1 p. 333 - 345
参考文献
Hann; Hudson
Journal of the American Chemical Society, 1942 , vol. 64, p. 2435,2436