3-甲基-1H-吲哚-2-甲醛合成路线 （共 33 条）
反应条件
tert-butylhypochlorite; water; triethylamine in tetrahydrofuran 1.5 h; Ambient temperature;
参考文献
Wilson, R. Marchall; Hengge, Alvan
Journal of Organic Chemistry, 1987 , vol. 52, # 13 p. 2699 - 2707
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in ethyl acetate 1 h; RefluxInert atmosphere;
参考文献
Dethe, Dattatraya H.; Erande, Rohan D.; Ranjan, Alok
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10106 - 10120
反应条件
2-Nitropropane; sodium ethanolate in ethanol T=20°C; 10 h;
参考文献
Mohanakrishnan, Arasambattu K.; Balamurugan, Ramalingam; Ramesh, Neelamegam
Tetrahedron Letters, 2005 , vol. 46, # 47 p. 8189 - 8193
反应条件
selenium(IV) oxide in 1,4-dioxane; water T=50°C; 4 h;
参考文献
Rodriguez; Lafuente; Garcia-Almaraz
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 5 p. 1281 - 1288
反应条件
trichlorophosphate T=100 - 120°C; Vilsmeier-Haack reaction; 3 h;
参考文献
Rodriguez; Lafuente; Garcia-Almaraz
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 5 p. 1281 - 1288
反应条件
Tl(Oac)3 in methanol T=25 - 30°C; 24 h;
参考文献
Banerji, Avijit; Ray, Rita; Pal, Sudhir C.; Banerji, Debasis; Maiti, Kaustabh K.
Journal of the Indian Chemical Society, 1998 , vol. 75, # 10-12 p. 698 - 704
反应条件
1: 59 percent / benzene / 24 h / 60 °C 2: 99 percent / tert-butyl hypochlorite, Et3N, H2O / tetrahydrofuran / 1.5 h / Ambient temperature View Scheme
参考文献
Banerji, Avijit; Ray, Rita; Pal, Sudhir C.; Banerji, Debasis; Maiti, Kaustabh K.
Journal of the Indian Chemical Society, 1998 , vol. 75, # 10-12 p. 698 - 704
反应条件
1: 82 percent / tin(IV) chloride / CH2Cl2 / 1.) -78 deg C up to -10 deg C, 2 h 2: 19 percent / potassium hydroxide / 0.75 h / Heating View Scheme
参考文献
Benzies, David W.M.; Fresneda, Pilar Martinez; Jones, R. Alan
Synthetic Communications, 1986 , vol. 16, # 14 p. 1799 - 1808
反应条件
1: 68 percent / sodium amalgam, Na2HPO4 / H2O; CH2Cl2 / 24 h 2: 54 percent / manganese dioxide / CH2Cl2 / 12 h View Scheme
参考文献
Dethe, Dattatraya H.; Erande, Rohan D.; Ranjan, Alok
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10106 - 10120
反应条件
acetyl chloride anschliessend mit Phosphor(V)-chlorid und Behandeln des gebildeten Saeurechlorids mit Lithium-<tri-tert-butoxy-alanat> in O,O'-Dimethyl-diaethylenglykol bei -70grad;
参考文献
Gore, Vivek; Gravel, Sylvie; Cossette, Chantal; Patel, Pranav; Chourey, Shishir; Ye, Qiuji; Rokach, Joshua; Powell, William S.
Journal of Medicinal Chemistry, 2014 , vol. 57, # 2 p. 364 - 377
