2,3-二氢-1H-吲哚-4-胺合成路线 （共 7 条）
反应条件
sulfuric acid T=170°C; 24 h;
参考文献
Tanaka; Murakami; Aizawa; Torii
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 11 p. 3742 - 3744
反应条件
1: 94 percent / Et4NOTs / dimethylformamide / 0.83 h / Ambient temperature; 3.3 mAcm-2 2: 86 percent / H2 / Raney Ni (W-2) / methanol / 2 h / 55 - 65 °C / 3800 - 6840 Torr 3: 92 percent / aq. 30percent H2SO4 / 24 h / 170 °C View Scheme
参考文献
Tanaka; Murakami; Aizawa; Torii
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 11 p. 3742 - 3744
反应条件
1: 86 percent / H2 / Raney Ni (W-2) / methanol / 2 h / 55 - 65 °C / 3800 - 6840 Torr 2: 92 percent / aq. 30percent H2SO4 / 24 h / 170 °C View Scheme
参考文献
Tanaka; Murakami; Aizawa; Torii
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 11 p. 3742 - 3744
反应条件
phosphoric acid T=220°C; 24 h; variation of concentration of H3PO4; Product distribution;
参考文献
Tanaka; Murakami; Aizawa; Torii
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 11 p. 3742 - 3744
反应条件
palladium on activated charcoal in xylene 3 h; Heating;
参考文献
Tanaka; Murakami; Aizawa; Torii
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 11 p. 3742 - 3744
反应条件
1: 86 percent / aq. 30percent H3PO4 / 24 h / 220 °C 2: 88 percent / 10percent Pd/C / o-xylene / 2.3 h / Heating View Scheme
参考文献
Tanaka; Murakami; Aizawa; Torii
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 11 p. 3742 - 3744
反应条件
phosphoric acid
T=220°C; 24 h;
参考文献
Tanaka; Murakami; Aizawa; Torii
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 11 p. 3742 - 3744
