2,3,5-三-O-苄基-D-阿拉伯呋喃糖-1-(4-硝基苯甲酸酯)合成路线 (共 11 条)
反应条件
pyridine in dichloromethane Ambient temperature;
参考文献
Kadir, Kamaliah; Mackenzie, Grahame; Shaw, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2304 - 2309
反应条件
sodium borohydride in methanol; dichloromethane; water; isopropyl alcohol; acetonitrile
参考文献
Berlex Biosciences Inc.
Patent: US5180824 A1, 1993 ;
反应条件
sodium borohydride in methanol; dichloromethane; water; isopropyl alcohol; acetonitrile
参考文献
Berlex Biosciences Inc.
Patent: US5180824 A1, 1993 ;
反应条件
sodium borohydride in methanol; dichloromethane; water; isopropyl alcohol; acetonitrile
反应条件
1: hydrogen chloride / CH2Cl2 / 0.17 h / 0 °C 2: 3.5 g / triethylamine / acetonitrile / 1.25 h 3: 1.8 g / phosphoryl chloride, triethylamine / CHCl3 / 2 h / Heating 4: 0.2 g / boron trichloride / CH2Cl2 / 2 h / Ambient temperature 5: 68 percent / ammonia / ethanol / 6 h / 150 °C View Scheme
参考文献
Kadir, Kamaliah; Mackenzie, Grahame; Shaw, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2304 - 2309
反应条件
sodium borohydride in methanol; dichloromethane; water; isopropyl alcohol; acetonitrile
反应条件
hydrogenchloride in dichloromethane T=0°C; 0.166667 h;
参考文献
Kadir, Kamaliah; Mackenzie, Grahame; Shaw, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2304 - 2309
反应条件
hydrogen bromide in dichloromethane
参考文献
Seela, Frank; Winkeler, Heinz-Dieter
Carbohydrate Research, 1983 , vol. 118, p. 29 - 36
反应条件
1: HCl / CH2Cl2 / 2 h / 0 °C
2: triethylamine / acetonitrile / 1 h / Heating
3: 25 percent / 1 M boron trichloride / CH2Cl2 / 64 h / -78 °C
View Scheme
参考文献
Bartlett; Cook; Holman; McComas; Nowoswait; Poonian; Baird-Lambert; Baldo; Marwood
Journal of Medicinal Chemistry, 1981 , vol. 24, # 8 p. 947 - 954
反应条件
hydrogenchloride in dichloromethane
T=0°C; 2 h;
参考文献
Doboszewski, Bogdan
Nucleosides, Nucleotides and Nucleic Acids, 2009 , vol. 28, # 10 p. 875 - 901