2-(1-甲基-1H-吡咯-2-基)吡啶合成路线 （共 12 条）
反应条件
hydrogenchloride; zinc
参考文献
Wibaut; Oosterhuis
Recueil des Travaux Chimiques des Pays-Bas, 1933 , vol. 52, p. 941,942
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Oosterhuis; Wibaut
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 729,734
反应条件
potassium phosphate; palladium diacetate; 2-dicyclohexylphosphino-1,1'-biphenyl in 1-methyl-pyrrolidin-2-one
T=15 - 125°C; 24.25 h; Inert atmosphere;
参考文献
Nadres, Enrico T.; Lazareva, Anna; Daugulis, Olafs
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 471 - 483
反应条件
[1,4-bis-(diphenylphosphine)butane]palladium (II) dichloride in tetrahydrofuran
1.5 h; Heating;
参考文献
Minato, Akio; Tamao, Kohei; Hayashi, Tamio; Suzuki, Keizo; Kumuda, Makoto
Tetrahedron Letters, 1981 , vol. 22, # 52 p. 5319 - 5322
参考文献
Savoia; Concialini; Roffia; Tarsi
Journal of Organic Chemistry, 1991 , vol. 56, # 5 p. 1822 - 1827
反应条件
1: 1.) t-BuLi 2.) MgBr2 / 1.) THF, pentane -78 and 25 deg C, 30 min. 2.) room temp., 1 h
2: 71 percent / PdCl2<1,4-bis(diphenylphosphino)butane> / tetrahydrofuran / 1.5 h / Heating
View Scheme
参考文献
Minato, Akio; Tamao, Kohei; Hayashi, Tamio; Suzuki, Keizo; Kumuda, Makoto
Tetrahedron Letters, 1981 , vol. 22, # 52 p. 5319 - 5322
反应条件
1: 80 percent / sodium acetate / ethanol / 24 h / Ambient temperature
2: 29 percent / toluene / 6 h / Heating
View Scheme
参考文献
Mullen, George B.; Georgiev, Vassil St.
Journal of Organic Chemistry, 1989 , vol. 54, # 10 p. 2476 - 2478
反应条件
potassium carbonate in dichloromethane
10 h; Ambient temperatureIrradiation;
参考文献
Seki, Koh-ichi; Ohkura, Kazue; Terashima, Masanao; Kanaoka, Yuichi
Heterocycles, 1984 , vol. 22, # 10 p. 2347 - 2350
反应条件
in toluene
6 h; Heating;
参考文献
Mullen, George B.; Georgiev, Vassil St.
Journal of Organic Chemistry, 1989 , vol. 54, # 10 p. 2476 - 2478
反应条件
diethyl ether
T=100°C;
参考文献
Wibaut; Dingemanse
Verslag van de Gewone Vergadering van de Afdeling Natuurkunde, Koninklijke Nederlandse Akademie van Wetenschappen, vol. 32, p. 287
Chem. Zentralbl., 1923 , vol. 94, # III p. 926
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Wibaut; Dingemanse
Recueil des Travaux Chimiques des Pays-Bas, 1923 , vol. 42, p. 1041
Chem. Zentralbl., 1923 , vol. 94, # III p. 926
反应条件
potassium carbonate in dichloromethane
10 h; Ambient temperatureIrradiation;
参考文献
Seki, Koh-ichi; Ohkura, Kazue; Terashima, Masanao; Kanaoka, Yuichi
Heterocycles, 1984 , vol. 22, # 10 p. 2347 - 2350
