N-(2-丙酰苯基)乙酰胺合成路线 (共 10 条)
反应条件
trichlorophosphate 1.) 0 deg C, 30 min, 2.) room temperature, 1 h, 3.) 90 deg C, 4 h;
参考文献
Amaresh; Perumal
Synthetic Communications, 1997 , vol. 27, # 2 p. 337 - 343
参考文献
Wohnlich
Archiv der Pharmazie (Weinheim, Germany), 1913 , vol. 251, p. 549
反应条件
1: With hydrogenchloride; ethanol; water T=40°C; 48 h; 2: With sodium carbonate in water pH=7;
参考文献
Boehringer Ingelheim International GmbH
Patent: EP1598343 A1, 2005 ;
Location in patent: Page/Page column 51 ;
反应条件
1: sulfuric acid; nitric acid / -10 °C 2: aqueous hydrochloric acid View Scheme
参考文献
Keneford et al.
Journal of the Chemical Society, 1948 , p. 358,359
Journal of the Chemical Society, 1950 , p. 1110,1111
反应条件
1: aqueous acetic acid; bromine 2: aqueous hydrochloric acid View Scheme
参考文献
Journal of Organic Chemistry, , vol. 11, p. 405,412
反应条件
triethylamine in tetrahydrofuran
参考文献
Tokunaga, Teruhisa; Hume, William Ewan; Kitoh, Makoto; Nagata, Ryu
Patent: US2003/181496 A1, 2003 ;
反应条件
(NH4)2S2O8; palladium (II) trifluoroacetate in diethylene glycol dimethyl ether
T=20°C;
参考文献
Fang, Ping; Li, Mingzong; Ge, Haibo
Journal of the American Chemical Society, 2010 , vol. 132, # 34 p. 11898 - 11899
反应条件
manganese(IV) oxide in dichloromethane
T=20°C; 72 h;
参考文献
Boehringer Ingelheim International GmbH
Patent: EP1598343 A1, 2005 ;
Location in patent: Page/Page column 51 ;
反应条件
1: tin; concentrated hydrochloric acid
View Scheme
参考文献
Wohnlich
Archiv der Pharmazie (Weinheim, Germany), 1913 , vol. 251, p. 549
参考文献
Wohnlich
Archiv der Pharmazie (Weinheim, Germany), 1913 , vol. 251, p. 549