4-碘-2-甲基-1-硝基苯合成路线 （共 12 条）
反应条件
2: Raney nickel; ethanol / 60 °C / Hydrogenation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 70, p. 2223,2228
反应条件
potassium acetate; triphenylphosphine; palladium dichloride T=110°C; Stille Cross Coupling; 1 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Davan, Elham Etemadi; Rostami, Abed; Nematollahi, Arash
Journal of Organometallic Chemistry, 2013 , vol. 740, p. 123 - 130
反应条件
1: potassium permanganate; tetrabutylammomium bromide 2: hydrogen; palladium on activated charcoal View Scheme
参考文献
Dong, Kui-Kui; Zhou, Hua-Hong; Guo, A-Rong; Chen, Tian; Wang, Yu-Liang
Asian Journal of Chemistry, 2013 , vol. 25, # 2 p. 1039 - 1042
反应条件
ammonia; water; iron(II) sulfate T=60 - 70°C;
参考文献
Artmann
Monatshefte fuer Chemie, 1905 , vol. 26, p. 1103
反应条件
potassium permanganate; tetrabutylammomium bromide
参考文献
Dong, Kui-Kui; Zhou, Hua-Hong; Guo, A-Rong; Chen, Tian; Wang, Yu-Liang
Asian Journal of Chemistry, 2013 , vol. 25, # 2 p. 1039 - 1042
参考文献
Lu Valle et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 2223,2228
反应条件
1: NH3; water; FeSO4 / 60 - 70 °C
2: diethyl ether
View Scheme
参考文献
Artmann
Monatshefte fuer Chemie, 1905 , vol. 26, p. 1103
反应条件
1: 110 °C
2: Raney nickel; ethanol / 60 °C / Hydrogenation
View Scheme
参考文献
Lu Valle et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 2223,2228
参考文献
Brown; Fried
Journal of the American Chemical Society, 1943 , vol. 65, p. 1841,1844
反应条件
1: With sulfuric acid; sodium nitrite in water
T=0°C; 0.166667 h;
2: With potassium iodide in water
T=0 - 20°C; 3.66667 h;
参考文献
Bao, Chunyan; Jin, Ming; Li, Bo; Xu, Yaodong; Jin, Jingyan; Zhu, Linyong
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 27 p. 5238 - 5244
