3-乙氧基羰基-1-苯基戊烷-1,4-二酮合成路线 （共 29 条）
反应条件
1: 72 percent / 12 M hydrochloric acid / ethanol / 24 h / Heating 2: 76 percent / lithium aluminum hydride / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Porretta; Scalzo; Chimenti; Bolasco; Biava; Fischetti; Riccardi
Farmaco, Edizione Scientifica, 1987 , vol. 42, # 5 p. 629 - 639
反应条件
1: toluene-4-sulphonic acid monohydrate / ethanol / 16 h / |Inert atmosphere; |Reflux 2: potassium hydroxide / ethanol; water / |Reflux View Scheme
参考文献
Krizaj, David; Prestwich, Glenn D.; Barabas, Peter; Xu, Yong; Ryskamp, Daniel
Patent: US2013/303539 A1, 2013 ;
参考文献
Borsche; Menz
Chemische Berichte, 1908 , vol. 41, p. 195
反应条件
in acetic acid T=80°C; 1 h; Heating;
参考文献
Petruso, S.; Caronna, S.; Sferlazzo, M.; Sprio, V.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 5 p. 1277 - 1280
反应条件
[BMIm][HSO4] T=150°C; Paal-Knorr pyrrole synthesis; 3 h;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 66, # 2 p. 191 - 196
反应条件
1: 63 percent / acetic acid / 0.33 h / Heating 2: 1.) 6 N HCl, sodium nitrite, 2.) hypophosphorous acid / 1.) water, 0 deg C, 0.5 h, 2.) water, RT, overnight View Scheme
参考文献
Cirrincione, Girolamo; Dattolo, Gaetano; Almerico, Anna Maria; Presti, Giuseppe; Aiello, Enrico
Heterocycles, 1986 , vol. 24, # 12 p. 3403 - 3410
反应条件
silica gelsupported polyphosphoric acid T=80°C; 1 h;
参考文献
Aoyama, Tadashi; Nagaoka, Takashi; Takido, Toshio; Kodomari, Mitsuo
Synthesis, 2011 , # 4 art. no. F18910SS, p. 619 - 625
反应条件
[BMIm][HSO4] T=150°C; Paal-Knorr furan synthesis; 3 h; Sealed tubeNeat (no solvent);
参考文献
Wang, Gangqiang; Guan, Zhi; Tang, Rongchang; He, Yanhong
Synthetic Communications, 2010 , vol. 40, # 3 p. 370 - 377
参考文献
Cusmano; Giambrone
Gazzetta Chimica Italiana, 1948 , vol. 78, p. 630,636
Full Text Show Details
Cusmano; Massara
Gazzetta Chimica Italiana, 1938 , vol. 68, p. 566,568
反应条件
sodium carbonate in methanol; water 6 h; Heating;
参考文献
Mackay, Donald; Dao, Le H.; Dust, Julian M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2408 - 2416
