2,3,5,6-四氟甲苯合成路线 （共 14 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane
反应条件
hydrogenchloride; zinc in water; N,N-dimethyl-formamide T=55°C; 8 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 36, # 10 p. 1488 - 1499
反应条件
hydrogenchloride; zinc in water; N,N-dimethyl-formamide T=50°C; 8 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 36, # 10 p. 1488 - 1499
反应条件
1: N2H4*H2O / dioxane / Heating 2: aq. CuSO4 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 31, p. 746 - 749
反应条件
1: 78 percent / zinc; conc. hydrochloric acid / dimethylformamide; H2O / 8 h / 55 °C 2: 15 percent / zinc; conc. hydrochloric acid / dimethylformamide; H2O / 8 h / 50 °C View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 36, # 10 p. 1488 - 1499
反应条件
potassium methanolate in ammonia T=-40 - -33°C; 4 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 5 p. 960 - 967
Zhurnal Organicheskoi Khimii, , vol. 20, # 5 p. 1055 - 1063
参考文献
Journal of Organic Chemistry, , vol. 31, p. 746 - 749
反应条件
1: 4-chloro-2,3,5,6-tetrafluorotoluene With zinc in N,N-dimethyl-formamide 6 h; Heating; 2: 3-chloroprop-1-ene With copper(l) chloride in N,N-dimethyl-formamide Further stages.;
参考文献
Russian Journal of Organic Chemistry, , vol. 44, # 1 p. 95 - 102
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, p. 2271 - 2276
Zhurnal Organicheskoi Khimii, , vol. 23, # 12 p. 2574 - 2580
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
参考文献
Imperial Chemical Industries PLC
Patent: US4370346 A1, 1983 ;
