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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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52249-82-8
合成路线
（共 17 条）
52249-82-8
→
反应条件
912957-28-9
反应条件
1: 71 percent / n-BuLi / tetrahydrofuran 2: 73 percent / H2 / Pd/C View Scheme
参考文献
Su, Chung-Ren; Shen, Yuh-Chiang; Kuo, Ping-Chung; Leu, Yann-Lii; Damu, Amooru G.; Wang, Yea-Hwey; Wu, Tian-Shung
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 24 p. 6155 - 6160
1835-11-6
4-苄氧基-3-甲氧基苯乙酮
+
52249-82-8
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反应条件
912957-28-9
反应条件
1: potassium hydroxide / methanol; water / 24.5 h / 0 - 20 °C 2: palladium 10 on activated carbon; hydrogen / methanol; ethyl acetate / 72 h / 20 °C View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
855242-15-8
+
68-12-2
N,N-二甲基甲酰胺
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反应条件
52249-82-8
+
1357024-85-1
反应条件
1: With trichlorophosphate T=0 - 80°C; 3.5 h; 2: Vilsmeier formylation;
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
42528-81-4
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反应条件
52249-82-8
反应条件
1: 50percent KOH 2: POCl3 / Ambient temperature 3: 3.7 g / H2 / Pd/C / ethyl acetate / 0.5 h / 760 Torr 4: 50percent KOH View Scheme
参考文献
Iinuma; Matoba; Tanaka; Mizuno
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 4 p. 1656 - 1662
52249-84-0
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反应条件
52249-82-8
反应条件
1: 3.7 g / H2 / Pd/C / ethyl acetate / 0.5 h / 760 Torr 2: 50percent KOH View Scheme
参考文献
Iinuma; Matoba; Tanaka; Mizuno
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 4 p. 1656 - 1662
6274-74-4
→
反应条件
52249-82-8
反应条件
1: POCl3 / Ambient temperature 2: 3.7 g / H2 / Pd/C / ethyl acetate / 0.5 h / 760 Torr 3: 50percent KOH View Scheme
参考文献
Iinuma; Matoba; Tanaka; Mizuno
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 4 p. 1656 - 1662
855242-15-8
+
68-12-2
N,N-二甲基甲酰胺
→
反应条件
52249-82-8
反应条件
trichlorophosphate
参考文献
Su, Chung-Ren; Shen, Yuh-Chiang; Kuo, Ping-Chung; Leu, Yann-Lii; Damu, Amooru G.; Wang, Yea-Hwey; Wu, Tian-Shung
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 24 p. 6155 - 6160
708-76-9
4,6-二甲氧基水杨醛
→
反应条件
52249-82-8
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 80 °C 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C 3: sodium hydroxide / methanol / 3 h / 20 °C 4: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C 5: trichlorophosphate / 3.5 h / 0 - 80 °C View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
1357024-84-0
→
反应条件
52249-82-8
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C 2: trichlorophosphate / 3.5 h / 0 - 80 °C View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
54917-02-1
→
反应条件
52249-82-8
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C 2: sodium hydroxide / methanol / 3 h / 20 °C 3: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C 4: trichlorophosphate / 3.5 h / 0 - 80 °C View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
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