5-甲基-5H-二苯并(b,f)氮杂卓合成路线 （共 17 条）
反应条件
sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid in dichloromethane 4.5 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 5 p. 1221 - 1230
反应条件
Fe(III)TPPCl; sodium dithionite; air; tetreamethyl ammonium hydroxide in methanol; dichloromethane; water 0.333333 h; Ambient temperature;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 32, # 3 p. 1252 - 1255
反应条件
sodium hydroxide; [N2224][Br] in dichloromethane; water
23 h;
参考文献
Gozlan; Halpern; Rabinovitz; et al.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, # 6 p. 1569 - 1671
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in toluene
T=100°C; 1 h; Schlenk techniqueInert atmosphere;
参考文献
Matsuda, Takanori; Sato, Shinya
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3329 - 3335
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
参考文献
Zheng, Zhizhen Barbara; Dowd, Paul
Tetrahedron Letters, 1993 , vol. 34, # 48 p. 7709 - 7712
参考文献
Ohta; Miyata; Hirobe
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1221 - 1230
反应条件
1: 100 percent / SOCl2
2: 86 percent
3: 89 percent
4: 63 percent / NaBH4
5: 44 percent / NaH / tetrahydrofuran / 16 h / Ambient temperature
6: 68 percent / Bu3SnH, AIBN / benzene / Heating
7: 88 percent / 50percent KOH / ethanol
8: 48 percent / DDQ
View Scheme
参考文献
Zheng, Zhizhen Barbara; Dowd, Paul
Tetrahedron Letters, 1993 , vol. 34, # 48 p. 7709 - 7712
反应条件
1: 86 percent
2: 89 percent
3: 63 percent / NaBH4
4: 44 percent / NaH / tetrahydrofuran / 16 h / Ambient temperature
5: 68 percent / Bu3SnH, AIBN / benzene / Heating
6: 88 percent / 50percent KOH / ethanol
7: 48 percent / DDQ
View Scheme
参考文献
Zheng, Zhizhen Barbara; Dowd, Paul
Tetrahedron Letters, 1993 , vol. 34, # 48 p. 7709 - 7712
反应条件
1: 89 percent
2: 63 percent / NaBH4
3: 44 percent / NaH / tetrahydrofuran / 16 h / Ambient temperature
4: 68 percent / Bu3SnH, AIBN / benzene / Heating
5: 88 percent / 50percent KOH / ethanol
6: 48 percent / DDQ
View Scheme
参考文献
Zheng, Zhizhen Barbara; Dowd, Paul
Tetrahedron Letters, 1993 , vol. 34, # 48 p. 7709 - 7712
反应条件
1: 63 percent / NaBH4
2: 44 percent / NaH / tetrahydrofuran / 16 h / Ambient temperature
3: 68 percent / Bu3SnH, AIBN / benzene / Heating
4: 88 percent / 50percent KOH / ethanol
5: 48 percent / DDQ
View Scheme
参考文献
Zheng, Zhizhen Barbara; Dowd, Paul
Tetrahedron Letters, 1993 , vol. 34, # 48 p. 7709 - 7712
