1: 4-(2-propenoxy)phenol With sodium hydride in tetrahydrofuran T=0°C; 0.333333 h; Inert atmosphere; 2: epichlorohydrin in tetrahydrofuran T=0 - 20°C; Inert atmosphereReflux;

1.1: potassium carbonate / N,N-dimethyl-formamide / 22 h / Reflux; Inert atmosphere 2.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere 2.2: 0 - 20 °C / Inert atmosphere; Reflux View Scheme

chloroform

T=18 - 20°C;