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52205-01-3
合成路线
(共 5 条)
52205-01-3
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反应条件
20795-53-3
3-苯基环己酮
反应条件
1: triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere 2: [RhCl(η2:η2-cycloocta-1,5-diene)]2; potassium hydroxide / 1,4-dioxane / 20 °C View Scheme
参考文献
Allen, Joseph C.; Kociok-Koehn, Gabriele; Frost, Christopher G.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 1 p. 32 - 35
52205-01-3
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
1: potassium hydroxide / toluene / 4 h / |Reflux; |Dean-Stark; |Inert atmosphere 2: methanol / 2 h / 0 - 20 °C / |Inert atmosphere 3: palladium diacetate; biphenyl-2-yl-di-tert-butyl-phosphane / N,N-dimethyl-formamide; water / 22 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Sakashita, Shohei; Takizawa, Miho; Sugai, Juugaku; Ito, Hajime; Yamamoto, Yasunori
Organic Letters, 2013 , vol. 15, # 17 p. 4308 - 4311
52205-01-3
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
1: triethylamine / tetrahydrofuran / 18 h / 0 - 20 °C / |Inert atmosphere 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol / 18 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Goggins, Sean; Rosevere, Eleanor; Bellini, Clement; Allen, Joseph C.; Marsh, Barrie J.; Mahon, Mary F.; Frost, Christopher G.
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 1 p. 47 - 52
52205-01-3
→
反应条件
61198-49-0
反应条件
1: triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere 2: [RhCl(η2:η2-cycloocta-1,5-diene)]2; potassium hydroxide / 1,4-dioxane / 20 °C View Scheme
参考文献
Allen, Joseph C.; Kociok-Koehn, Gabriele; Frost, Christopher G.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 1 p. 32 - 35
52205-01-3
→
反应条件
3976-34-9
1,3-二甲基-2-苯基苯
反应条件
1: potassium hydroxide / toluene / 4 h / |Reflux; |Dean-Stark; |Inert atmosphere 2: methanol / 2 h / 0 - 20 °C / |Inert atmosphere 3: palladium diacetate / N,N-dimethyl-formamide; water / 22 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Sakashita, Shohei; Takizawa, Miho; Sugai, Juugaku; Ito, Hajime; Yamamoto, Yasunori
Organic Letters, 2013 , vol. 15, # 17 p. 4308 - 4311