5-乙酰基-6-甲基-2(1H)-吡啶酮合成路线 （共 12 条）
反应条件
in N,N-dimethyl-formamide 1) RT, 3.5 h, 2) reflux, 24 h;
参考文献
Singh, Baldev; Lesher, George Y.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 7 p. 2085 - 2091
反应条件
in various solvent(s) 3 h; Heating;
参考文献
Yamanaka; Miyake; Suda; Ohhara; Ogawa
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 6 p. 1556 - 1567
反应条件
palladium on activated charcoal T=250°C; 0.333333 h;
参考文献
Kato, Tetsuzo; Sato, Masayuki; Wagai, Akihiro
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 603 - 606
反应条件
1: 49 percent / 50percent H2SO4 / 7.5 h / Heating 2: 78 percent / various solvent(s) / 3 h / Heating View Scheme
参考文献
Mosti, Luisa; Schenone, Pietro; Menozzi, Giulia
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1503 - 1509
反应条件
1: 91 percent / ethanol / 24 h / Ambient temperature 2: 75 percent / aq. H2SO4 / 2 h / 50 °C 3: 70 percent / 6N hydrochloric acid / 10 h / Heating 4: 60 percent / Cu powder / quinoline / 1 h / Heating View Scheme
参考文献
Mosti, Luisa; Schenone, Pietro; Menozzi, Giulia
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1503 - 1509
反应条件
1: 84 percent / ethanol / 24 h / Ambient temperature 2: 75 percent / aq. H2SO4 / 2 h / 50 °C 3: 70 percent / 6N hydrochloric acid / 10 h / Heating 4: 60 percent / Cu powder / quinoline / 1 h / Heating View Scheme
参考文献
Mosti, Luisa; Schenone, Pietro; Menozzi, Giulia
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1503 - 1509
反应条件
1: 70 percent / 6N hydrochloric acid / 10 h / Heating 2: 60 percent / Cu powder / quinoline / 1 h / Heating View Scheme
参考文献
Mosti, Luisa; Schenone, Pietro; Menozzi, Giulia
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1503 - 1509
反应条件
1: 94 percent / ammonium acetate / toluene / 5 h / Heating 2: 62 percent / dimethylformamide / 1) RT, 3.5 h, 2) reflux, 24 h View Scheme
参考文献
Singh, Baldev; Lesher, George Y.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 7 p. 2085 - 2091
反应条件
1: 60 percent / acetonitrile / Ambient temperature 2: 10 percent / 2.5 h / 600 °C / 0 - 0.01 Torr View Scheme
参考文献
Derbyshire, Paul A.; Hunter, Gordon A.; McNab, Hamish; Monahan, Lilian C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 17 p. 2017 - 2026
反应条件
1: 74 percent / NBS, benzoyl peroxide / CCl4 / 8 h / Heating 2: 90 percent / dioxane / 5 h / Heating 3: 64 percent / AcONH4 / dimethylformamide / 5 h / Heating View Scheme
参考文献
Singh, Baldev; Pennock, Patrick O.; Lesher, George Y.; Bacon, Edward R.; Page, Donald F.
Heterocycles, 1993 , vol. 36, # 1 p. 133 - 144
