3-氨基-2-环己烯-1-酮合成路线 （共 56 条）
反应条件
ammonium acetate; ethyl orthosilicate in ethanol Heating;
参考文献
Zhao, Yuanhong; Zhao, Jingfeng; Zhou, Yongyun; Lei, Ze; Li, Liang; Zhang, Hongbin
New Journal of Chemistry, 2005 , vol. 29, # 6 p. 769 - 772
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=60°C; P=760.051 Torr; 14 h; Green chemistry; TemperatureTime;
参考文献
Sajiki, Hironao; Ikawa, Takashi; Hirota, Kosaku
Organic Process Research and Development, 2005 , vol. 9, # 2 p. 219 - 220
反应条件
ammonium acetate; acetic acid in benzene 0.3 h; Heating;
参考文献
Baraldi, P. G.; Simoni, D.; Manfredini, S.
Synthesis, 1983 , # 11 p. 902 - 903
参考文献
E. I. Du Pont de Nemours and Company
Patent: US5149874 A1, 1992 ;
反应条件
phosphoric acid; hydrogen
参考文献
E. I. Du Pont de Nemours and Company
Patent: US5149874 A1, 1992 ;
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; P=760.051 Torr; 23 h; Green chemistry;
参考文献
Sajiki, Hironao; Ikawa, Takashi; Hirota, Kosaku
Organic Process Research and Development, 2005 , vol. 9, # 2 p. 219 - 220
反应条件
pyridine in N,N-dimethyl-formamide T=80°C; 10 h; Yield given;
参考文献
Torii, Sigeru; Inokuchi, Tsutomu; Kubota, Minoru
Synthesis, 1986 , # 5 p. 400 - 402
反应条件
1: 91 percent / 6 h / Heating 2: 85 percent / AcCl; NaCNBH3; HCl / methanol / 6 h / pH 4 / Heating View Scheme
参考文献
LeBel, Norman A.; Caprathe, Bradley W.
Journal of Organic Chemistry, 1985 , vol. 50, # 20 p. 3938 - 3940
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide 18 h; Heating;
参考文献
Synthetic Communications, , vol. 28, # 7 p. 1197 - 1200
反应条件
in N,N-dimethyl-formamide 12 h; Ambient temperature;
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 9 p. 2736 - 2746
