(R)-(+)-1-(2-萘基)乙醇合成路线 （共 65 条）
反应条件
sodium carbonate in toluene T=40°C; 72 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Kato, Katsuya; Irimescu, Roxana; Saito, Takao; Yokogawa, Yoshiyuki; Takahashi, Haruo
Bioscience, Biotechnology and Biochemistry, 2003 , vol. 67, # 1 p. 203 - 206
反应条件
(mer-[(S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene(1-)]Ru(CO)Cl)2(ZnCl2); hydrogen; sodium methylate in isopropyl alcohol T=40°C; P=22801.5 Torr; 24 h; Inert atmosphereAutoclave; optical yield given as percent eeenantioselective reaction;
参考文献
Ito, Jun-Ichi; Teshima, Tomoki; Nishiyama, Hisao
Chemical Communications, 2012 , vol. 48, # 8 p. 1105 - 1107
反应条件
tricarbonyl(η6-arene)chromium(0) complex derived from (1S,2R)-N,N-dibutylnorephedrine in hexane; toluene T=0°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Huang, Wei-Sheng; Hu, Qiao-Sheng; Pu, Lin
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 7940 - 7956
反应条件
sodium formate; chiral monosulfonamide-cyclohexane-1,2-diamine-RhCp* complex in water T=40°C; 2 h;
参考文献
Cortez, Norma A.; Aguirre, Gerardo; Parra-Hake, Miguel; Somanathan, Ratnasamy
Tetrahedron Letters, 2007 , vol. 48, # 25 p. 4335 - 4338
反应条件
(1R,2R)-α,α,α',α'-tetraphenyl-1,2-cyclohexanedimethanol; TiF4 in CH3CN 1) THF, hexane, 0 deg C to RT, 20 min, 2) THF, hexane, 20 min, 3) THF, hexane, -10 deg C, 12 h then warm to RT; Yield givenMultistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Alegre, Sabina; Dieguez, Montserrat; Pmies, Oscar
Tetrahedron Asymmetry, 2011 , vol. 22, # 8 p. 834 - 839
反应条件
2-exo-morpholinoisobornane-10-thiol in hexane T=20°C; 48 h; Inert atmosphere; enantioselective reaction;
参考文献
Cheng, Ying-Ni; Wu, Hsyueh-Liang; Wu, Ping-Yu; Shen, Ying-Ying; Uang, Biing-Jiun
Chemistry - An Asian Journal, 2012 , vol. 7, # 12 p. 2921 - 2924
反应条件
1: With succinic acid anhydride; Candida antarctica lipase B in diethyl ether T=20°C; Enzymatic reaction; 2: With sodium hydroxide in water
参考文献
Bouzemi, Nassima; Debbeche, Hanane; Aribi-Zouioueche, Louisa; Fiaud, Jean-Claude
Tetrahedron Letters, 2004 , vol. 45, # 3 p. 627 - 630
反应条件
Candida antarctica lipase B in diethyl ether T=20°C; Enzymatic reaction;
参考文献
Bouzemi, Nassima; Debbeche, Hanane; Aribi-Zouioueche, Louisa; Fiaud, Jean-Claude
Tetrahedron Letters, 2004 , vol. 45, # 3 p. 627 - 630
反应条件
(1R)-N-oxyl-1-(N-benzylcarbamoyl)-8-azabicyclo[3.2.1]octane; sodium hydrogencarbonate; sodium bromide in dichloromethane; water T=0°C; Electrochemical reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Demizu, Yosuke; Shiigi, Hirofumi; Mori, Hiroyuki; Matsumoto, Kazuya; Onomura, Osamu
Tetrahedron Asymmetry, 2008 , vol. 19, # 23 p. 2659 - 2665
反应条件
1: With bis(acetylacetonate)nickel(II); C41H61O8P in tetrahydrofuran T=5°C; 3 h; Inert atmosphere; 2: With hydrogenchloride; water in tetrahydrofuran Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Alegre, Sabina; Dieguez, Montserrat; Pmies, Oscar
Tetrahedron Asymmetry, 2011 , vol. 22, # 8 p. 834 - 839
