1: 1) lithium diisopropylamide / 1) THF, -78 deg C, 30 min; 2) 1 h at -78 deg C to room temp.
2: CH2Cl2 / -78 deg C -> room temperature
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参考文献
Hannaby, Malcolm; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 303 - 311
(i) LDA, THF, (ii) /BRN= 639794/; Multistep reaction;
参考文献
Seebach,D.; Teschner,M.
Chemische Berichte, 1976 , vol. 109, p. 1601 - 1616
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Trost,B.M. et al.
Journal of the American Chemical Society, 1976 , vol. 98, p. 4887 - 4902