9-(环氧-2-甲基)-9H-咔唑合成路线 (共 10 条)
反应条件
potassium hydroxide; tetrabutylammomium bromide; potassium carbonate in toluene T=105 - 106°C; 0.166667 h; microwave irradiation;
参考文献
Bogdal; Lukasiewicz; Pielichowski; Bednarz
Synthetic Communications, 2005 , vol. 35, # 23 p. 2973 - 2983
反应条件
1: dibenzopyrrole With potassium hydroxide in N,N-dimethyl-formamide T=20°C; 1 h; 2: (R/S)-2-Bromomethyl-oxirane in N,N-dimethyl-formamide T=20°C; 20 h; Cooling with ice;
参考文献
Bersot, Ross; Humphries, Paul
Patent: US2013/303524 A1, 2013 ;
Location in patent: Paragraph 0254-0255 ;
反应条件
phosphoric acid; sulfuric acid; dihydrogen peroxide; sodium tungstate; Aliquatreg; 336 in water; 1,2-dichloro-ethane T=70°C; pH=1.6; 1 h; microwave irradiation;
参考文献
Bogdal; Lukasiewicz; Pielichowski; Bednarz
Synthetic Communications, 2005 , vol. 35, # 23 p. 2973 - 2983
反应条件
potassium hydroxide in acetone
参考文献
Lubczak, Renata
Heterocyclic Communications, 2006 , vol. 12, # 3-4 p. 201 - 208
参考文献
Esrielew; Larin
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 791
engl. Ausg. S. 905
反应条件
sulfuric acid in water; acetone pH=1;
参考文献
Lubczak, Renata
Heterocyclic Communications, 2006 , vol. 12, # 3-4 p. 201 - 208
反应条件
in ethanol
0.5 h; Heating;
参考文献
Mysyk, D. D.; Dolzhenko, A. T.; Kononova, R. E.; Charfas, O. V.; Galat, V. F.
Pharmaceutical Chemistry Journal, 1984 , vol. 18, # 4 p. 266 - 268
Khimiko-Farmatsevticheskii Zhurnal, 1984 , vol. 18, # 4 p. 449 - 451
参考文献
Mysyk, D. D.; Dolzhenko, A. T.; Kononova, R. E.; Charfas, O. V.; Galat, V. F.
Pharmaceutical Chemistry Journal, 1984 , vol. 18, # 4 p. 266 - 268
Khimiko-Farmatsevticheskii Zhurnal, 1984 , vol. 18, # 4 p. 449 - 451
参考文献
Mysyk, D. D.; Dolzhenko, A. T.; Kononova, R. E.; Charfas, O. V.; Galat, V. F.
Pharmaceutical Chemistry Journal, 1984 , vol. 18, # 4 p. 266 - 268
Khimiko-Farmatsevticheskii Zhurnal, 1984 , vol. 18, # 4 p. 449 - 451
参考文献
Mysyk, D. D.; Dolzhenko, A. T.; Kononova, R. E.; Charfas, O. V.; Galat, V. F.
Pharmaceutical Chemistry Journal, 1984 , vol. 18, # 4 p. 266 - 268
Khimiko-Farmatsevticheskii Zhurnal, 1984 , vol. 18, # 4 p. 449 - 451