1-(2-异丙基苯基)-2-硫脲合成路线 （共 13 条）
反应条件
potassium iodide; sulfuric acid; sodium sulfite; sodium nitrite in water; ethyl acetate
参考文献
C.I.R.D. Galderma
Patent: US5723499 A1, 1998 ;
反应条件
1: With sulfuric acid; sodium nitrite in water T=0 - 5°C; 2: With potassium iodide in water T=5°C; Reflux;
参考文献
Parik, Patrik; Kulhanek, Jiri; Ludwig, Miroslav; Wagner, Roman; Rotrekl, Ivan; Drahonovsky, Dusan; Meca, Ludek; Smidkova, Marketa; Tobrman, Tomas; Dvorak, Dalimil
Organometallics, 2010 , vol. 29, # 18 p. 4135 - 4138
反应条件
1,4-dioxane; sodium hydroxide; sodium hypobromide
参考文献
Sato
Bulletin of the Chemical Society of Japan, 1959 , vol. 32, p. 1130
参考文献
Willgerodt; Jahn
Justus Liebigs Annalen der Chemie, 1911 , vol. 385, p. 328
参考文献
Gore,P.H. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973 , p. 2940 - 2948
反应条件
1: (i) NaNO2, aq. H2SO4, (ii) KI 2: aq. NaOH View Scheme
参考文献
Gore,P.H. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973 , p. 2940 - 2948
参考文献
Edinger; Goldberg
Chemische Berichte, 1900 , vol. 33, p. 2884
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Grahl
Chemische Berichte, 1895 , vol. 28, p. 89
反应条件
sulfuric acid in methanol; ethyl acetate
参考文献
C.I.R.D. Galderma
Patent: US5723499 A1, 1998 ;
反应条件
sulfuric acid Heating;
参考文献
Blaszykowski, Christophe; Aktoudianakis, Evangelos; Bressy, Cyril; Alberico, Dino; Lautens, Mark
Organic Letters, 2006 , vol. 8, # 10 p. 2043 - 2045
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl-formamide T=150°C; 0.5 h; Microwave irradiation;
参考文献
GLAXO GROUP LIMITED
Patent: WO2007/147109 A2, 2007 ;
Location in patent: Page/Page column 180-181 ;
WO 2007/147109 A2
