2-溴-４-硝基吡啶氮氧化物合成路线 （共 24 条）
反应条件
chloroformic acid ethyl ester in 1,2-dichloro-ethane T=40 - 65°C;
参考文献
Journal of Heterocyclic Chemistry, , vol. 48, # 4 p. 961 - 964
反应条件
acetyl-bromide in acetic acid T=80°C;
参考文献
Garcia-Lago, Ramon; Alonso-Gomez, Jose-Lorenzo; Sicre, Cristina; Cid, Maria-Magdalena
Heterocycles, 2008 , vol. 75, # 1 p. 57 - 64
反应条件
in ethanol
T=70 - 80°C; 16 h;
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
反应条件
in ethanol
T=70 - 80°C; 3 h;
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
反应条件
1: 56 percent / ethanol / 16 h / 70 - 80 °C
2: 70 percent / 2 h / Heating
View Scheme
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
反应条件
1: 56 percent / ethanol / 16 h / 70 - 80 °C
2: 70 percent / 2 h / Heating
3: 70 percent / H2O / 7 h / 120 - 130 °C
View Scheme
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
反应条件
1: 69 percent / ethanol / 3 h / 70 - 80 °C
2: 52 percent / 2 h / Heating
3: 69 percent / H2O / 120 - 130 °C
View Scheme
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
反应条件
1: 69 percent / ethanol / 3 h / 70 - 80 °C
2: 52 percent / 2 h / Heating
3: 69 percent / H2O / 120 - 130 °C
4: 47 percent / PCl3 / CHCl3 / 22 h / Heating
View Scheme
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
反应条件
1: 73 percent / ethanol / 1 h / 70 - 80 °C
2: 73 percent / 2 h / Heating
3: 84 percent / H2O / 120 - 130 °C
4: 73 percent / PCl3 / CHCl3 / 22 h / Heating
View Scheme
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
反应条件
1: 69 percent / ethanol / 3 h / 70 - 80 °C
2: 52 percent / 2 h / Heating
View Scheme
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
