苯甲酸3-甲基2-丁烯酯合成路线 （共 15 条）
反应条件
1: in dichloromethane T=20°C; 2: With poly{trans-bicyclo[2.2.1]hept-5-ene-2,3-di(chlorocarbonyl)} in dichloromethane Heating;
参考文献
Moore, Joel D.; Byrne, Robert J.; Vedantham, Punitha; Flynn, Daniel L.; Hanson, Paul R.
Organic Letters, 2003 , vol. 5, # 23 p. 4241 - 4244
反应条件
potassium carbonate in dichloromethane 70 h; Ambient temperature;
参考文献
Badet, Bernard; Julia, Marc; Ramirez-Munoz, Miguel
Synthesis, 1980 , # 11 p. 926 - 929
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane Ambient temperature;
参考文献
Fleming, Ian; Higgins, Dick; Lawrence, Nicholas J.; Thomas, Andrew P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3331 - 3350
反应条件
in dichloromethane T=20°C; 72 h;
参考文献
Badet, B.; Julia, M.; Ramirez-Munoz, M.; Sarrazin, C. A.
Tetrahedron, 1983 , vol. 39, # 19 p. 3111 - 3126
反应条件
in acetone 4 h; Photolysis; Title compound not separated from byproducts;
参考文献
Canadian Journal of Chemistry, , vol. 79, # 2 p. 114 - 120
反应条件
pyridine; phenyl isocyanate in benzene 15 h; Ambient temperature;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 1 p. 5 - 10
反应条件
1: 95 percent / Zn; HOAc / 0.5 h / 60 °C 2: 10 percent / acetone / 4 h / Photolysis View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 79, # 2 p. 114 - 120
反应条件
1: 59 percent / O3 / CH2Cl2 / -70 °C 2: pyridine, PhNCO / benzene / 15 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 1 p. 5 - 10
反应条件
1: 59 percent / O3 / CH2Cl2 / -70 °C 2: pyridine, PhNCO / benzene / 15 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 1 p. 5 - 10
反应条件
n-butyllithium 1.) Et2O, hexane, -20 deg C, 15 min., 2.) 1 h, 3.) room temp., overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 403, # 1.2 p. 49 - 62
